{"id":86693,"date":"2017-06-17T06:30:07","date_gmt":"2017-06-16T22:30:07","guid":{"rendered":"http:\/\/www.cailiaoniu.com\/?p=86693"},"modified":"2017-06-18T12:05:07","modified_gmt":"2017-06-18T04:05:07","slug":"nano-energy-%e5%85%b7%e6%9c%89%e5%85%89%e7%94%9f%e7%94%b5%e5%ad%90%e4%bf%98%e8%8e%b7%e7%a7%af%e7%b4%af%e4%bd%8d%e7%82%b9%e5%92%8c%e8%be%93%e8%bf%90%e9%80%9a%e9%81%93%e7%bb%93%e6%9e%84%e7%9a%84","status":"publish","type":"post","link":"http:\/\/www.cailiaoniu.com\/?p=86693","title":{"rendered":"Nano Energy: \u5177\u6709\u5149\u751f\u7535\u5b50\u4fd8\u83b7\/\u79ef\u7d2f\u4f4d\u70b9\u548c\u8f93\u8fd0\u901a\u9053\u7ed3\u6784\u7684\u9ad8\u6548\u5149\u50ac\u5316\u5242\u7684\u6784\u5efa"},"content":{"rendered":"

\u3010\u5f15\u8a00\u3011<\/strong><\/span><\/p>\n

\u5149\u50ac\u5316\u6548\u7387\u53d6\u51b3\u4e8e\u5149\u751f\u8f7d\u6d41\u5b50\u7684\u6fc0\u53d1\u3001\u5149\u751f\u7535\u5b50\u7a7a\u7a74\u5bf9\u7684\u5206\u79bb\u548c\u4f20\u8f93\u3001\u6d3b\u6027\u4f4d\u70b9\u4e0a\u7684\u6c27\u5316\u8fd8\u539f\u53cd\u5e94\u8fd9\u4e09\u4e2a\u8fc7\u7a0b\u7684\u534f\u540c\u4f5c\u7528\u3002\u9488\u5bf9\u5149\u50ac\u5316\u5242\u7684\u6ce2\u8c31\u54cd\u5e94\u8303\u56f4\u548c\u6c27\u5316\u8fd8\u539f\u80fd\u529b\u76f8\u4e92\u8026\u5408\uff0c\u5448\u73b0\u51fa\u76f8\u53cd\u7684\u53d8\u5316\u8d8b\u52bf\u7684\u95ee\u9898\uff0c\u4eba\u4eec\u901a\u5e38\u9009\u62e9\u9ad8\u6d3b\u6027\u534a\u5bfc\u4f53\u4e0e\u8f83\u7a84\u5e26\u9699\u7684\u534a\u5bfc\u4f53\u8026\u5408\u65b9\u5f0f\u6765\u63d0\u9ad8\u5149\u50ac\u5316\u5242\u5149\u50ac\u5316\u6027\u80fd\uff0c\u4f46\u7a84\u5e26\u9699\u534a\u5bfc\u4f53\u7684\u5149\u50ac\u5316\u5f80\u5f80\u6d3b\u6027\u76f8\u5bf9\u8f83\u4f4e\uff0c\u56e0\u6b64\u964d\u4f4e\u4e86\u5149\u50ac\u5316\u5242\u5149\u50ac\u5316\u53cd\u5e94\u6d3b\u6027\u4f4d\u70b9\u5bc6\u5ea6\u3002\u5229\u7528\u8d35\u91d1\u5c5e\u7684\u7b49\u79bb\u6fc0\u5143\u5171\u632f\u6548\u5e94\uff0c\u53ef\u5c06\u8d35\u91d1\u5c5e\/\u5bbd\u5e26\u9699\u5149\u50ac\u5316\u5242\u5f02\u8d28\u7ed3\u6784\u7684\u5149\u5438\u6536\u8303\u56f4\u62d3\u5c55\u5230\u53ef\u89c1\u5149\u533a\u57df\u3002\u4f46\u662f\u7531\u4e8e\u5f02\u8d28\u7ed3\u6784\u4e2d\u5b58\u5728\u5149\u751f\u8f7d\u6d41\u5b50\u7684\u968f\u673a\u4f20\u8f93\uff0c\u56e0\u6b64\u5355\u4e00\u7684\u8d35\u91d1\u5c5e\/\u534a\u5bfc\u4f53\u7684\u5f02\u8d28\u7ed3\u6784\u96be\u4ee5\u6ee1\u8db3\u63d0\u9ad8\u5149\u751f\u8f7d\u6d41\u5b50\u5206\u79bb\u7684\u9700\u6c42\u3002\u56e0\u6b64\u9009\u7528\u80fd\u5e26\u5339\u914d\u7684\u534a\u5bfc\u4f53\u91d1\u5c5e\u6750\u6599\uff0c\u8bbe\u8ba1\u534a\u5bfc\u4f53-\u8d35\u91d1\u5c5e-\u534a\u5bfc\u4f53\u7684\u5149\u50ac\u5316\u7ed3\u6784\uff0c\u6784\u5efa\u5149\u751f\u7535\u5b50\u7684\u5b9a\u5411\u8f93\u8fd0\uff0c\u63d0\u9ad8\u5149\u751f\u7535\u5b50-\u7a7a\u7a74\u7684\u5206\u79bb\u662f\u6700\u7ec8\u5236\u5907\u51fa\u9ad8\u6027\u80fd\u7684\u5149\u50ac\u5316\u5242\u7684\u91cd\u8981\u9014\u5f84\u3002<\/p>\n

\u3010\u6210\u679c\u7b80\u4ecb\u3011<\/strong><\/span><\/p>\n

\u8fd1\u65e5\uff0c\u91cd\u5e86\u5927\u5b66\u80e1\u9648\u679c\u6559\u6388\u8bfe\u9898\u7ec4\u4ece\u9ad8\u6d3b\u6027\u7684\u5bbd\u5e26\u9699\u6750\u6599SrSO4<\/sub>\u5165\u624b\uff0c\u5229\u7528Ag\u7eb3\u7c73\u9897\u7c92\u7b49\u79bb\u6fc0\u5143\u5171\u632f\u5438\u6536\u6765\u62d3\u5c55\u5438\u6536\u8c31\u8303\u56f4\uff0c\u5efa\u7acb\u6709\u5149\u751f\u7535\u5b50\u8f93\u8fd0\u901a\u9053\u7684SrSO4<\/sub>\/Ag\/TiO2<\/sub>\u53cc\u5f02\u8d28\u7ed3\u6784\uff0c\u5e76\u5b9e\u73b0\u5149\u751f\u7535\u5b50\u7a7a\u7a74\u5bf9\u7684\u6709\u6548\u5206\u79bb\uff0c\u6781\u5927\u63d0\u9ad8\u4e86\u5149\u50ac\u5316\u6548\u7387\u3002\u5229\u7528\u4e8c\u6c27\u5316\u949b\u548c\u786b\u9178\u9536\u80fd\u5e26\u5339\u914d\u7684\u4f18\u52bf\uff0c\u7ed3\u5408Ag\u7eb3\u7c73\u9897\u7c92\u5bf9\u5149\u751f\u7535\u5b50\u7684\u4fd8\u83b7\u3001\u50a8\u84c4\u4f5c\u7528\u548c\u5176\u7b49\u79bb\u6fc0\u5143\u5171\u632f\u6548\u5e94\uff0c\u6210\u529f\u5b9e\u73b0\u4e86\u5149\u751f\u7535\u5b50\u4ece\u4e8c\u6c27\u5316\u949b\u2192\u94f6\u2192\u786b\u9178\u9536\u7684\u5b9a\u5411\u8f93\u8fd0\uff0c\u6781\u5927\u63d0\u9ad8\u5149\u751f\u8f7d\u6d41\u5b50\u7684\u5206\u79bb\u6548\u7387\u3002\u7531\u4e8e\u5929\u9752\u77f3\u7ed3\u6784\u7684\u786b\u9178\u9536\u5bf9\u6eb6\u6db2\u79bb\u5b50\u8f83\u5f3a\u7684\u5438\u9644\u80fd\u529b\u548c\u8f83\u9ad8\u7684\u5149\u50ac\u5316\u53cd\u5e94\u6d3b\u6027\uff0c\u6700\u7ec8\u5b9e\u73b0SrSO4<\/sub>\/Ag\/TiO2<\/sub>\u6709\u4f18\u5f02\u7684\u5149\u50ac\u5316\u964d\u89e3\u6c61\u67d3\u7269\u4e9a\u7532\u57fa\u84dd(MB)\u548c\u5149\u5206\u89e3\u6c34\u4ea7\u6c22\u6027\u80fd\u3002\u672c\u9879\u5de5\u4f5c\u5236\u5907\u4e86\u5149\u50ac\u5316\u6027\u80fd\u4f18\u5f02\u7684\u5149\u50ac\u5316\u5242\uff0c\u62d3\u5bbd\u4e86\u5149\u50ac\u5316\u5242\u7684\u7814\u7a76\u8303\u56f4\uff0c\u4e3a\u5efa\u7acb\u5149\u751f\u8f7d\u6d41\u5b50\u7684\u8f93\u8fd0\u901a\u9053\u3001\u64cd\u63a7\u5149\u751f\u8f7d\u6d41\u5b50\u7684\u8f93\u8fd0\u884c\u4e3a\u63d0\u4f9b\u4e86\u65b0\u601d\u8def\u3002<\/p>\n

\u3010\u56fe\u6587\u5bfc\u8bfb\u3011<\/strong><\/span><\/p>\n

\u56fe<\/strong>1 <\/strong>\u50ac\u5316\u5242\u7269\u76f8\u4e0e\u5f62\u8c8c\u5206\u6790<\/strong><\/span><\/p>\n

\"\"<\/p>\n

(a) SrTiO3<\/sub>\u7eb3\u7c73\u7acb\u65b9\u5757\uff1b<\/p>\n

(b) Ag\/TiO2\uff1b<\/sub><\/p>\n

(c) SrSO4<\/sub>\/TiO2<\/sub> SEM \u56fe\uff1b<\/p>\n

(d) TiO2<\/sub>\/Ag\/SrSO4<\/sub> TEM\u56fe\uff1b<\/p>\n

(e-f)TiO2<\/sub>\/Ag\/SrSO4 <\/sub>\u9ad8\u5206\u8fa8TEM\u56fe\uff1b<\/p>\n

(g)XRD\u56fe\u3002<\/p>\n

\u91c7\u7528\u4e09\u6b65\u9aa4\u5408\u6210TiO2<\/sub>\/Ag\/SrSO4<\/sub>\uff0c\u9996\u5148\u5236\u5907\u949b\u9178\u9536\u7eb3\u7c73\u7acb\u65b9\u5757\uff0c\u7136\u540e\u52a0\u786b\u9178\u5236\u5907\u6210SrSO4<\/sub>\/TiO2<\/sub>\u5f02\u8d28\u7ed3\uff0c\u7136\u540e\u91c7\u7528\u5149\u8fd8\u539f\u65b9\u6cd5\u5728\u5176\u8868\u9762\u6c89\u79ef\u94f6\uff0c\u5236\u5907\u51fa\u4e0d\u540cAg\u542b\u91cf\u7684TiO2<\/sub>\/Ag\/SrSO4<\/sub>\u5f02\u8d28\u7ed3\u6784\u3002\u4e3a\u6bd4\u8f83\u5176\u5149\u50ac\u5316\u6027\u80fd\uff0c\u540c\u65f6\u5236\u5907Ag\/TiO2<\/sub>\u5149\u50ac\u5316\u5242\u3002<\/p>\n

\u56fe<\/strong>2 <\/strong>\u50ac\u5316\u5242\u5149\u50ac\u5316\u6027\u80fd\u53ca\u673a\u7406\u793a\u610f\u56fe<\/strong><\/span><\/p>\n

\"\"<\/p>\n

(a)\u5149\u50ac\u5316\u964d\u89e3\u4e9a\u7532\u57fa\u84dd\uff1b<\/p>\n

(b)\u4e0d\u540cR(R=TiO2<\/sub>\/SrSO4<\/sub>:Ag)\u7684\u5149\u50ac\u5316\u5242TiO2<\/sub>\/Ag\/SrSO4<\/sub>\u964d\u89e3\u4e9a\u7532\u57fa\u84dd\u7684\u5faa\u73af\u7279\u6027\uff1b<\/p>\n

(c)R=16:1\u7684\u5149\u50ac\u5316\u5242\u5149\u50ac\u5316\u964d\u89e3\u4e9a\u7532\u57fa\u84dd\u7684\u5faa\u73af\u7279\u6027\uff1b<\/p>\n

(d)SrSO4<\/sub>\u3001TiO2<\/sub>\u548cAg\u7684\u80fd\u5e26\u56fe\uff1b<\/p>\n

(e) TiO2<\/sub>\/Ag\/SrSO4<\/sub>\u7684\u5149\u751f\u7535\u5b50\u4f20\u8f93\u793a\u610f\u56fe\u3002<\/p>\n

\u9996\u5148\u5c0620 mg\u5149\u50ac\u5316\u5242\u572850 mL MB (10-5<\/sup> mol\u00b7L-1<\/sup>)\u6eb6\u6db2\u4e2d\u907f\u5149\u6405\u62cc30\u5206\u949f\uff0c\u7136\u540e\u518d\u7528\u6a21\u62df\u592a\u9633\u5149\u7167\u5c04\u3002\u5b9e\u9a8c\u7ed3\u679c\u8868\u660e\u76f8\u5bf9\u4e8eAg\/TiO2<\/sub>, TiO2<\/sub>\/Ag\/SrSO4<\/sub>\u7684\u5149\u964d\u89e3\u65f6\u95f4\u7f29\u77ed\u4e00\u534a\uff0c\u6027\u80fd\u8fdc\u4f18\u8d8a\u4e8eTiO2<\/sub>\u7eb3\u7c73\u9897\u7c92\u548cTiO2<\/sub>\/SrSO4<\/sub>\uff1b\u907f\u5149\u5b9e\u9a8c\u8868\u660e\u7531\u5149\u50ac\u5316\u5242TiO2<\/sub>\/Ag\/SrSO4<\/sub>\u5bf9MB\u7684\u5438\u9644\u800c\u5f15\u8d77MB\u6d53\u5ea6\u964d\u4f4e\u7684\u4f5c\u7528\u975e\u5e38\u5fae\u5f31\uff1b4\u6b21\u5faa\u73af\u5149\u964d\u89e3MB\u5b9e\u9a8c\u8868\u660e\u5149\u50ac\u5316\u5242\u6709\u4f18\u5f02\u7684\u7a33\u5b9a\u6027\u3002\u6839\u636e\u6587\u732e\u53caMott\u2013Schottky\u6d4b\u8bd5\u5f97\u5230\u4e8c\u6c27\u5316\u949b\u3001\u94f6\u548c\u786b\u9178\u9536\u7684\u80fd\u5e26\u7ed3\u6784\uff0c\u63d0\u51fa\u5149\u751f\u7535\u5b50\u5b9a\u5411\u8f93\u8fd0\u7684\u6a21\u578b\u3002<\/p>\n

\u56fe<\/strong>3 <\/strong>\u5149\u50ac\u5316\u5242\u5149\u50ac\u5316\u5206\u89e3\u6c34\u6027\u80fd\u53ca\u673a\u7406\u793a\u610f\u56fe<\/strong><\/span><\/p>\n

\"\"<\/p>\n

(a)SrSO4<\/sub>\u7684\uff08110\uff09\u548c\uff08210\uff09\u9762\u7684\u6676\u4f53\u7ed3\u6784\uff1b<\/p>\n

(b) SrSO4<\/sub>\u7684Zeta\u7535\u4f4d\uff1b<\/p>\n

(c) TiO2<\/sub>\/Ag\/SrSO4<\/sub>(R=16\uff1a1)\u5149\u50ac\u5316\u5206\u89e3\u6c34\u7684\u5faa\u73af\u6d4b\u8bd5\u3002<\/p>\n

\u4e3a\u63ed\u793aTiO2<\/sub>\/Ag\/SrSO4<\/sub>\u7ed3\u6784\u4e2d\u786b\u9178\u9536\u7684\u4f5c\u7528\uff0c\u5efa\u7acb\u786b\u9178\u9536\u7684\u6676\u683c\u7ed3\u6784\u53d1\u73b0\u5728\u5176\u89e3\u79bb\u9762\uff08110\uff09\u548c\uff08210\uff09\u5b58\u5728\u5927\u91cf\u786b\u9178\u6839\u79bb\u5b50\u548c\u9536\u79bb\u5b50\uff0c\u5bf9\u6eb6\u6db2\u4e2d\u79bb\u5b50\u6709\u5f3a\u5438\u9644\u4f5c\u7528\uff0cZeta\u7535\u4f4d\u6d4b\u8bd5\u9a8c\u8bc1\u4e86\u8fd9\u4e00\u601d\u60f3\u6b63\u786e\u6027\u3002\u56e0\u6b64\u786b\u9178\u9536\u5bf9\u6eb6\u6db2\u79bb\u5b50\u7684\u5f3a\u5438\u9644\u4f5c\u7528\u6781\u5927\u589e\u52a0\u5f3a\u6c27\u5316\u6027\u81ea\u7531\u57fa\u7684\u4ea7\u751f\u51e0\u7387\uff0c\u6709\u52a9\u4e8e\u5149\u50ac\u5316\u6027\u80fd\u63d0\u9ad8\u300250\u6beb\u514b\u7684\u5149\u50ac\u5316\u5242\u7f6e\u4e8e80\u6beb\u5347\u542b20\u6beb\u5347\u7532\u9187\u6eb6\u6db2\u4e2d\uff0c\u7528300 W Xe \u706f\u4f5c\u5149\u6e90\u8f90\u71674\u5c0f\u65f6\u5f97\u5230\u5149\u50ac\u5316\u5206\u89e3\u6c34\u4ea7\u91cf\u4e3a260\u03bcmol\/(h.g)\uff0c\u662fP25\u4ea7\u91cf\u768419\u500d\uff0c\u8868\u660e\u53cc\u5f02\u8d28\u7ed3\u6784\u4e2d\u5149\u751f\u7535\u5b50\u8f93\u8fd0\u901a\u9053\u7684\u5efa\u7acb\u548c\u786b\u9178\u9536\u5bf9\u6c34\u6eb6\u6db2\u79bb\u5b50\u7684\u5438\u9644\u4f5c\u7528\u5171\u540c\u63d0\u9ad8\u4e86\u5176\u5149\u50ac\u5316\u6027\u80fd\u3002<\/p>\n

\u3010\u603b\u7ed3\u3011<\/strong><\/span><\/p>\n

\u53cc\u5f02\u8d28\u7ed3\u6784\u4e2d\u8f7d\u6d41\u5b50\u8f93\u8fd0\u901a\u9053\u7684\u5efa\u7acb\uff0c\u6781\u5927\u63d0\u9ad8\u5149\u751f\u8f7d\u6d41\u5b50\u7684\u5206\u79bb\uff0c\u63d0\u9ad8\u4e86\u4f53\u7cfb\u7684\u5149\u50ac\u5316\u6027\u80fd\uff0c\u4e3a\u5bbd\u5e26\u9699\u6750\u6599\u5728\u5149\u50ac\u5316\u9886\u57df\u7684\u5e94\u7528\u548c\u5149\u751f\u8f7d\u6d41\u5b50\u7684\u64cd\u63a7\u7814\u7a76\u63d0\u4f9b\u4e86\u65b0\u7684\u601d\u8def\u3002<\/span><\/p>\n

\u3010\u8bfe\u9898\u7ec4\u7b80\u4ecb\u3011<\/strong><\/span><\/p>\n

\u91cd\u5e86\u5927\u5b66\u7269\u7406\u5b66\u9662\u80e1\u9648\u679c\u8bfe\u9898\u7ec4\u7b80\u4ecb\uff1a\u4e3b\u8981\u7814\u7a76\u65b9\u5411\u4e3a\u80fd\u6e90\u6750\u6599\u548c\u80fd\u6e90\u5668\u4ef6\u3002\u5df2\u7ecf\u5f62\u6210\u4e86\u4ece\u6750\u6599\u751f\u957f\u5230\u5668\u4ef6\u5236\u5907\u7684\u5b8c\u6574\u4f53\u7cfb\uff0c\u5305\u62ec\u5bf9\u80fd\u91cf\u6536\u96c6\u5668\u4ef6\uff08\u57fa\u4e8e\u6469\u64e6\u7535\u3001\u538b\u7535\u548c\u70ed\u91ca\u7535\u7684\u7eb3\u7c73\u53d1\u7535\u673a\uff09\u3001\u8d85\u7ea7\u7535\u5bb9\u5668\u3001\u5149\u50ac\u5316\u3001\u71c3\u6599\u7535\u6c60\u3001\u592a\u9633\u80fd\u7535\u6c60\u3001\u4f20\u611f\u5668\u7b49\u7684\u7814\u7a76\u3002\u5df2\u53d1\u8868SCI\u6587\u7ae0210\u591a\u7bc7\uff0c\u88ab\u5f15\u75284200\u591a\u6b21 (Web of Science)\uff0c\u5176\u4e2d\uff0c\u5f71\u54cd\u56e0\u5b50\u5927\u4e8e10\u7684\u6587\u7ae0\u670922\u7bc7\uff0c\u53d1\u8868180 \u4f59\u7bc7\uff0cESI\u9ad8\u88ab\u5f15\u8bba\u65877\u7bc7\u3002\u7533\u8bf7\u53d1\u660e\u4e13\u522915\u9879\uff0c\u6388\u674315\u9879\u3002<\/p>\n

\"\"<\/p>\n

\u8bfe\u9898\u7ec4\u94fe\u63a5\uff1ahttp:\/\/phys.cqu.edu.cn\/about\/shizililiang\/2015-10-05\/162.html<\/a><\/p>\n

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