{"id":94836,"date":"2017-08-06T14:00:41","date_gmt":"2017-08-06T06:00:41","guid":{"rendered":"http:\/\/www.cailiaoniu.com\/?p=94836"},"modified":"2017-08-05T19:11:27","modified_gmt":"2017-08-05T11:11:27","slug":"adv-funct-mater-%ef%bc%9a%e5%85%b7%e6%9c%89%e7%a9%ba%e9%97%b4%e5%88%86%e7%a6%bb%e6%b4%bb%e6%80%a7%e4%bd%8d%e7%82%b9%e7%9a%84la2o3%e6%94%b9%e6%80%a7latio2n%e5%85%89%e5%82%ac%e5%8c%96%e5%89%82","status":"publish","type":"post","link":"http:\/\/www.cailiaoniu.com\/?p=94836","title":{"rendered":"Adv. Funct. Mater.\uff1a\u5177\u6709\u7a7a\u95f4\u5206\u79bb\u6d3b\u6027\u4f4d\u70b9\u7684La2O3\u6539\u6027LaTiO2N\u5149\u50ac\u5316\u5242\u52a9\u529b\u4e8c\u6c27\u5316\u78b3\u8fd8\u539f\u8fc7\u7a0b"},"content":{"rendered":"<p><strong>\u3010\u80cc\u666f\u4ecb\u7ecd\u3011<\/strong><\/p>\n<p>\u4f7f\u7528H<sub>2<\/sub>O\u4f5c\u4e3a\u8fd8\u539f\u5242\u5c06\u4e8c\u6c27\u5316\u78b3\u901a\u8fc7\u5149\u50ac\u5316\u8f6c\u5316\u4e3a\u9ad8\u9644\u52a0\u503c\u7684\u592a\u9633\u80fd\u71c3\u6599\u5df2\u88ab\u89c6\u4e3a\u53ef\u6301\u7eed\u80fd\u6e90\u672a\u6765\u53d1\u5c55\u7684\u91cd\u8981\u7b56\u7565\u3002\u4ece\u52a8\u529b\u5b66\u4e0a\u6765\u8bf4\uff0c\u6d3b\u5316\u4e8c\u6c27\u5316\u78b3\u5206\u5b50\u548c\u4fc3\u8fdb\u7f13\u6162\u7684\u6c34\u6c27\u5316\u91ca\u653e\u8d28\u5b50\u662f\u4e24\u4e2a\u91cd\u8981\u7684\u534a\u53cd\u5e94\u8fc7\u7a0b\uff0c\u52a0\u901f\u8fd9\u4e24\u4e2a\u53cd\u5e94\u8fc7\u7a0b\u7684\u8fdb\u884c\u53ef\u4ee5\u6709\u6548\u5730\u5b9e\u73b0\u5728\u592a\u9633\u80fd\u9a71\u52a8\u4e0b\u4e8c\u6c27\u5316\u78b3\u5230\u71c3\u6599\u7684\u8f6c\u53d8\u3002<\/p>\n<p><strong>\u3010\u6210\u679c\u7b80\u4ecb\u3011<\/strong><\/p>\n<p>\u8fd1\u65e5\uff0c\u6765\u81ea<strong>\u5357\u4eac\u5927\u5b66<\/strong>\u7684<strong>\u95eb\u4e16\u6210\u526f\u6559\u6388\uff08\u901a\u8baf\u4f5c\u8005\uff09<\/strong>\u7b49\u4eba\u63d0\u51fa\u4e86\u4e00\u79cd\u4f7f\u7528\u56fa\u4f53\u78b1\u6765\u4fee\u9970\u5177\u6709\u6c27\u7a7a\u4f4d\u7f3a\u9677\u7684\u5149\u50ac\u5316\u5242\u7684\u6709\u6548\u9014\u5f84\uff0c\u65e8\u5728\u540c\u65f6\u52a0\u901f\u4e24\u4e2a\u534a\u53cd\u5e94\u8fc7\u7a0b\u3002\u4e3a\u4e86\u9a8c\u8bc1\u8fd9\u4e00\u5047\u8bbe\uff0c\u5728\u5177\u6709\u6c27\u7a7a\u4f4d\u7684LaTiO<sub>2<\/sub>N\u7684\u8868\u9762\u4e0a\u4fee\u9970La<sub>2<\/sub>O<sub>3<\/sub><sub>\u00a0<\/sub>\u56fa\u6001\u78b1\uff0c\u5b9e\u73b0\u4e86\u4e8c\u6c27\u5316\u78b3\u8fd8\u539f\u8fc7\u7a0b\u4e2dCH<sub>4<\/sub>\u4ea7\u7387\u589e\u52a0\u4e24\u500d\u3002\u5176\u663e\u8457\u7684\u6548\u679c\u6765\u81ea\u4ee5\u4e0b\u4e24\u4e2a\u56e0\u7d20\uff1a\uff081\uff09La<sub>2<\/sub>O<sub>3<\/sub>\u4e2d\u4f5c\u4e3a\u78b1\u6027\u4f4d\u70b9\u7684O<sup>2-<\/sup>\u6709\u5229\u4e8eCO<sub>2<\/sub>\u4ee5CO<sub>3<\/sub><sup>2-<\/sup>\u5f62\u5f0f\u5316\u5b66\u5438\u9644\uff0c\u5927\u5927\u6709\u52a9\u4e8eO=C=O\u952e\u7684\u5f2f\u66f2\u548cCO<sub>2<\/sub>\u5206\u5b50\u7684\u6700\u4f4e\u672a\u5360\u636e\u5206\u5b50\u8f68\u9053\u80fd\u91cf\u7684\u964d\u4f4e\u3002\uff082\uff09LaTiO<sub>2<\/sub>N\u4e0a\u7684\u6c27\u7a7a\u4f4d\u6709\u5229\u4e8e\u6d3b\u5316H<sub>2<\/sub>O\u4e3a\u5438\u9644OH\uff0c\u4ece\u800c\u6709\u6548\u964d\u4f4e\u6c34\u6c27\u5316\u53cd\u5e94\u52bf\u5792\uff0c\u91ca\u653e\u51fa\u8d28\u5b50\u3002\u76f8\u5173\u6210\u679c\u4ee5\u9898\u4e3a\u201c<strong>La<sub>2<\/sub>O<sub>3<\/sub>-Modified LaTiO<sub>2<\/sub>N Photocatalyst with Spatially Separated Active Sites Achieving Enhanced CO2\u00a0Reduction<\/strong>\u201d\u53d1\u8868\u5728\u4e86<strong>Advanced Functional Materials<\/strong>\u4e0a\u3002<\/p>\n<p><strong>\u3010\u56fe\u6587\u5bfc\u8bfb\u3011<\/strong><\/p>\n<p><strong>\u56fe1 XRD\\SEM\\TEM\u5206\u6790<\/strong><\/p>\n<p><img loading=\"lazy\" decoding=\"async\" class=\"aligncenter size-full wp-image-94838\" src=\"http:\/\/www.cailiaoniu.com\/wp-content\/uploads\/2017\/08\/1-11.png\" alt=\"\" width=\"600\" height=\"406\" srcset=\"http:\/\/www.cailiaoniu.com\/wp-content\/uploads\/2017\/08\/1-11.png 600w, http:\/\/www.cailiaoniu.com\/wp-content\/uploads\/2017\/08\/1-11-300x203.png 300w\" sizes=\"(max-width: 600px) 100vw, 600px\" \/><\/p>\n<p>a\uff09La<sub>2<\/sub>TiO<sub>5<\/sub>\uff0cxLa<sub>2<\/sub>O<sub>3<\/sub>\/LaTiO<sub>2<\/sub>N\uff08x = 0.5,0.33,0.3\u548c0.16\uff09\u548c\u7eafLaTiO<sub>2<\/sub>N\u7684XRD\u56fe<\/p>\n<p>b\uff09La<sub>2<\/sub>TiO<sub>5<\/sub>\u7684SEM\u56fe\u50cf<\/p>\n<p>c-e\uff090.5La<sub>2<\/sub>O<sub>3<\/sub>\/LaTiO<sub>2<\/sub>\u7684c\uff09SEM\u56fe\u50cf\uff0cd\uff09TEM\u56fe\u50cf\uff0c\u4ee5\u53cae\uff09HR-TEM\u6676\u683c\u56fe\u50cf<\/p>\n<p>f\uff090.3La<sub>2<\/sub>O<sub>3<\/sub>\/LaTiO<sub>2<\/sub>\u7684HR-TEM\u6676\u683c\u56fe\u50cf<\/p>\n<p>g\uff09\u7eafLaTiO<sub>2<\/sub>N\u7684HR-TEM\u56fe\u50cf<\/p>\n<p><strong>\u56fe2 \u7d2b\u5916\u53ef\u89c1\u5438\u6536\u5149\u8c31\u53caXPS\u5149\u8c31\u5206\u6790<\/strong><\/p>\n<p><img loading=\"lazy\" decoding=\"async\" class=\"aligncenter size-full wp-image-94839\" src=\"http:\/\/www.cailiaoniu.com\/wp-content\/uploads\/2017\/08\/2-9.png\" alt=\"\" width=\"600\" height=\"485\" srcset=\"http:\/\/www.cailiaoniu.com\/wp-content\/uploads\/2017\/08\/2-9.png 600w, http:\/\/www.cailiaoniu.com\/wp-content\/uploads\/2017\/08\/2-9-300x243.png 300w\" sizes=\"(max-width: 600px) 100vw, 600px\" \/><\/p>\n<p>a\uff09\u5404\u79cdLaTiO<sub>2<\/sub>N\u6837\u54c1\u7684\u7d2b\u5916\u53ef\u89c1\u5438\u6536\u5149\u8c31<\/p>\n<p>b-d\uff09xLa<sub>2<\/sub>O<sub>3<\/sub>\/LaTiO<sub>2<\/sub>N\uff08x = 0.5\u548c0.3\uff09\u548c\u7eafLaTiO<sub>2<\/sub>N\u7684b\uff09EPR\uff0cc\uff09Ti 2p\uff0c\u548cd\uff09O 1s\u6838\u5fc3\u7ea7XPS\u5149\u8c31<\/p>\n<p><strong>\u56fe3 CH<sub>4<\/sub>\u4ea7\u7387\u5206\u6790<\/strong><\/p>\n<p><img loading=\"lazy\" decoding=\"async\" class=\"aligncenter size-full wp-image-94840\" src=\"http:\/\/www.cailiaoniu.com\/wp-content\/uploads\/2017\/08\/3-10.png\" alt=\"\" width=\"600\" height=\"232\" srcset=\"http:\/\/www.cailiaoniu.com\/wp-content\/uploads\/2017\/08\/3-10.png 600w, http:\/\/www.cailiaoniu.com\/wp-content\/uploads\/2017\/08\/3-10-300x116.png 300w\" sizes=\"(max-width: 600px) 100vw, 600px\" \/><\/p>\n<p>a\uff09\u5e26\u6709\u4e0d\u540c\u6469\u5c14\u91cfLa<sub>2<\/sub>O<sub>3<\/sub>\u7684LaTiO<sub>2<\/sub>N\u7684CH<sub>4<\/sub>\u4ea7\u7387\u4f5c\u4e3a\u7167\u5c04\u65f6\u95f4\u7684\u51fd\u6570<\/p>\n<p>b\uff09\u9664\u4e86\u7b2c\u4e00\u5c0f\u65f6\u4e4b\u5916\uff0c\u5728\u53e6\u59167\u5c0f\u65f6\u7167\u5c04\u4e0b\uff0c\u4e0d\u540c\u6469\u5c14\u91cf\u7684La<sub>2<\/sub>O<sub>3<\/sub>\u7684LaTiO<sub>2<\/sub>N\u5e73\u5747CH<sub>4<\/sub>\u4ea7\u7387<\/p>\n<p><strong>\u56fe4 FT-IR\u548cXPS\u5149\u8c31<\/strong><\/p>\n<p><img loading=\"lazy\" decoding=\"async\" class=\"aligncenter size-full wp-image-94841\" src=\"http:\/\/www.cailiaoniu.com\/wp-content\/uploads\/2017\/08\/4-9.png\" alt=\"\" width=\"600\" height=\"509\" srcset=\"http:\/\/www.cailiaoniu.com\/wp-content\/uploads\/2017\/08\/4-9.png 600w, http:\/\/www.cailiaoniu.com\/wp-content\/uploads\/2017\/08\/4-9-300x255.png 300w\" sizes=\"(max-width: 600px) 100vw, 600px\" \/><\/p>\n<p>a\uff09\u5728\u9ed1\u6697\u73af\u58832\u5c0f\u65f6\u540eCO<sub>2<\/sub>\u5438\u9644\u540e\u5149\u50ac\u5316\u5242\u7684FT-IR\u5149\u8c31<\/p>\n<p>b\uff09b\u5728\u9ed1\u6697\u73af\u5883\u4e2dCO<sub>2<\/sub>\u548cH<sub>2<\/sub>O\u5438\u9644\u540e\uff0c\u5149\u50ac\u5316\u5242\u7684C 1s\u82af\u80fd\u7ea7XPS\u5149\u8c31<\/p>\n<p>c,d\uff09\u5149\u50ac\u5316\u53cd\u5e94\u540e\u5149\u50ac\u5316\u5242\u7684C 1s\u548cd\uff09O 1\u82af\u80fd\u7ea7XPS\u5149\u8c31<\/p>\n<p><strong>\u56fe5 CO<sub>2<\/sub>\u548cH<sub>2<\/sub>O\u7684\u5438\u9644\u80fd<\/strong><\/p>\n<p><img loading=\"lazy\" decoding=\"async\" class=\"aligncenter size-full wp-image-94842\" src=\"http:\/\/www.cailiaoniu.com\/wp-content\/uploads\/2017\/08\/5-4.png\" alt=\"\" width=\"600\" height=\"291\" srcset=\"http:\/\/www.cailiaoniu.com\/wp-content\/uploads\/2017\/08\/5-4.png 600w, http:\/\/www.cailiaoniu.com\/wp-content\/uploads\/2017\/08\/5-4-300x146.png 300w\" sizes=\"(max-width: 600px) 100vw, 600px\" \/><\/p>\n<p>\u8ba1\u7b97\u51fa\u5177\u6709O<sub>Vs<\/sub>\u7684La<sub>2<\/sub>O<sub>3<\/sub>\uff08002\uff09\u548cLaTiO<sub>2<\/sub>N\uff08002\uff09\u7684\u80fd\u91cf\u5206\u522b\u4e3a-12174.0\u548c-6792.6eV<\/p>\n<p><strong>\u56fe6 \u901a\u8fc7H<sub>2<\/sub>O\u5c06CO<sub>2<\/sub>\u6c27\u5316\u548c\u8fd8\u539f\u6210CH<sub>4<\/sub>\u7684\u53ef\u80fd\u673a\u5236<\/strong><\/p>\n<p><img loading=\"lazy\" decoding=\"async\" class=\"aligncenter size-full wp-image-94843\" src=\"http:\/\/www.cailiaoniu.com\/wp-content\/uploads\/2017\/08\/6-4.png\" alt=\"\" width=\"600\" height=\"191\" srcset=\"http:\/\/www.cailiaoniu.com\/wp-content\/uploads\/2017\/08\/6-4.png 600w, http:\/\/www.cailiaoniu.com\/wp-content\/uploads\/2017\/08\/6-4-300x96.png 300w\" sizes=\"(max-width: 600px) 100vw, 600px\" \/><\/p>\n<p>\u663e\u7136\uff0c\u901a\u8fc7H<sub>2<\/sub>O\u5bf9La<sub>2<\/sub>O<sub>3<\/sub>\u6539\u6027\u7684LaTiO<sub>2<\/sub>N\u7684\u8fd8\u539f\u53cd\u5e94\u4e3b\u8981\u662f\u7531\u4e8eLa<sub>2<\/sub>O<sub>3<\/sub>\u7684\u6676\u683c\u4e2d\u7684O<sup>2-<\/sup>\u548cLaTiO<sub>2<\/sub>N\u4e0a\u7684O<sub>Vs<\/sub>\u80fd\u591f\u5c06CO<sub>2<\/sub>\u548cH<sub>2<\/sub>O\u6d3b\u5316\u6210CO<sub>3<\/sub><sup>2-<\/sup>\u548cH<sup>+<\/sup><\/p>\n<p><strong><sup>\u00a0<\/sup>\u3010\u603b\u7ed3\u3011<\/strong><\/p>\n<p>\u4e3a\u63d0\u9ad8\u5149\u50ac\u5316\u4e8c\u6c27\u5316\u78b3\u8f6c\u5316\u7387\uff0c\u8be5\u7814\u7a76\u63d0\u51fa\u4e86\u4f7f\u7528\u56fa\u4f53\u78b1\u548c\u6c27\u7a7a\u4f4d\u8c03\u63a7\u5149\u50ac\u5316\u6750\u6599\u50ac\u5316\u529f\u80fd\u7684\u65b9\u6cd5\uff0c\u65e8\u5728\u540c\u65f6\u52a0\u901f\u4e24\u4e2a\u91cd\u8981\u7684\u534a\u53cd\u5e94\u8fc7\u7a0b\u3002\u5728\u4e0d\u540c\u7a7a\u95f4\u4f4d\u7f6e\u540c\u65f6\u6d3b\u5316CO<sub>2<\/sub>\u548cH<sub>2<\/sub>O\u4ee5\u5b9e\u73b0\u901f\u7387\u5339\u914d\u7684\u534a\u53cd\u5e94\u901f\u7387\u53ef\u4ee5\u6291\u5236\u592a\u9633\u80fd\u8f6c\u6362\u7684\u9006\u5411\u53cd\u5e94\u3002<\/p>\n<p><strong>\u6587\u732e\u94fe\u63a5<\/strong>\uff1a<a href=\"http:\/\/onlinelibrary.wiley.com\/doi\/10.1002\/adfm.201702447\/full\" target=\"_blank\" rel=\"noopener\">La<sub>2<\/sub>O<sub>3<\/sub>-Modified LaTiO<sub>2<\/sub>N Photocatalyst with Spatially Separated Active ,Sites Achieving Enhanced CO2\u00a0Reduction<\/a>\uff08Adv. Funct. Mater.,2017,DOI: 10.1002\/adfm.201702447\uff09<\/p>\n<p style=\"font: 17px\/30px 'Lantinghei SC', 'Open Sans', Arial, 'Hiragino Sans GB', 'Microsoft YaHei', \u5fae\u8f6f\u96c5\u9ed1, STHeiti, 'WenQuanYi Micro Hei', SimSun, sans-serif; margin: 0px 0px 30px; padding: 0px; border: 0px currentColor; color: #000000; text-indent: 0px; letter-spacing: normal; vertical-align: baseline; background-color: #ffffff;\">\u672c\u6587\u7531\u6750\u6599\u4eba\u65b0\u80fd\u6e90\u7ec4Allen\u3010\u674e\u4f26\u3011\u4f9b\u7a3f\uff0c\u6750\u6599\u725b\u6574\u7406\u7f16\u8f91\u3002\u53c2\u4e0e\u65b0\u80fd\u6e90\u8bdd\u9898\u8ba8\u8bba\u8bf7\u52a0\u5165\u201c\u6750\u6599\u4eba\u65b0\u80fd\u6e90\u6750\u6599\u4ea4\u6d41\u7fa4 422065952\u201d\u3002<\/p>\n<p style=\"font: 17px\/30px 'Lantinghei SC', 'Open Sans', Arial, 'Hiragino Sans GB', 'Microsoft YaHei', \u5fae\u8f6f\u96c5\u9ed1, STHeiti, 'WenQuanYi Micro Hei', SimSun, sans-serif; margin: 0px 0px 30px; padding: 0px; border: 0px currentColor; color: #000000; text-indent: 0px; 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margin: 0px 0px 30px; padding: 0px; border: 0px currentColor; color: #000000; text-indent: 0px; letter-spacing: normal; vertical-align: baseline; background-color: #ffffff;\">\u6b22\u8fce\u5927\u5bb6\u5230\u6750\u6599\u4eba\u5ba3\u4f20\u79d1\u6280\u6210\u679c\u5e76\u5bf9\u6587\u732e\u8fdb\u884c\u6df1\u5165\u89e3\u8bfb\uff0c\u6295\u7a3f\u90ae\u7bb1tougao@cailiaoren.com\u3002<\/p>\n<p style=\"font: 17px\/30px 'Lantinghei SC', 'Open Sans', Arial, 'Hiragino Sans GB', 'Microsoft YaHei', \u5fae\u8f6f\u96c5\u9ed1, STHeiti, 'WenQuanYi Micro Hei', SimSun, sans-serif; margin: 0px 0px 30px; padding: 0px; border: 0px currentColor; color: #000000; text-indent: 0px; letter-spacing: normal; vertical-align: baseline; background-color: #ffffff;\"><strong style=\"margin: 0px; padding: 0px; border: 0px currentColor; font-family: 'Lantinghei SC', 'Open Sans', Arial, 'Hiragino Sans GB', 'Microsoft YaHei', \u5fae\u8f6f\u96c5\u9ed1, STHeiti, 'WenQuanYi Micro Hei', SimSun, sans-serif; font-size: 17px; font-weight: 600; 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