{"id":95179,"date":"2017-08-09T06:30:50","date_gmt":"2017-08-08T22:30:50","guid":{"rendered":"http:\/\/www.cailiaoniu.com\/?p=95179"},"modified":"2017-08-07T22:20:50","modified_gmt":"2017-08-07T14:20:50","slug":"%e3%80%90%e6%9c%aa%e5%9b%9e%e5%a4%8d%e3%80%91nano-energy%ef%bc%9a%e5%8f%af%e7%a7%bb%e6%a4%8d%e6%80%a7%e5%af%8clif%e4%bf%9d%e6%8a%a4%e5%b1%82%e7%a8%b3%e5%ae%9ali-%e7%94%b5%e8%a7%a3%e6%b6%b2%e7%95%8c","status":"publish","type":"post","link":"http:\/\/www.cailiaoniu.com\/?p=95179","title":{"rendered":"Nano Energy\uff1a\u53ef\u79fb\u690d\u6027\u5bccLiF\u4fdd\u62a4\u5c42\u7a33\u5b9aLi \/\u7535\u89e3\u6db2\u754c\u9762\uff0c\u6539\u5584Li\u91d1\u5c5e\u7535\u6c60\u5faa\u73af\u7a33\u5b9a\u6027"},"content":{"rendered":"

\u3010\u5f15\u8a00\u3011<\/strong><\/p>\n

\u4e3a\u4e86\u8fbe\u5230\u9502\u79bb\u5b50\u7535\u6c60\uff08LIBs\uff09\u7684\u7406\u8bba\u80fd\u91cf\u5bc6\u5ea6\uff0c\u5145\u5206\u5b9e\u73b0\u80fd\u6e90\u5229\u7528\uff0c\u5f00\u53d1\u65b0\u578b\u9ad8\u80fd\u91cf\u5bc6\u5ea6\u7684\u7535\u6781\u6750\u6599\u548c\u7535\u6c60\u4f53\u7cfb\u4ecd\u8feb\u5728\u7709\u776b\u3002\u4f5c\u4e3a\u76ee\u524d\u6700\u7406\u60f3\u7684\u8d1f\u6781\u6750\u6599\uff0c\u9502\u91d1\u5c5e\u5177\u5907\u8d85\u9ad8\u7684\u7406\u8bba\u5bb9\u91cf\uff083860 mAh\/g\uff09\u548c\u8f83\u4f4e\u7684\u6c27\u5316\u8fd8\u539f\u7535\u4f4d\uff08(-3.040 V vs. \u6807\u51c6\u6c22\u7535\u6781\uff09\uff0c\u5728\u5b9e\u9645\u5e94\u7528\u4e2dLi\u91d1\u5c5e\u4e0d\u4ec5\u53ef\u4ee5\u63d0\u9ad8\u4f20\u7edf\u7535\u6c60\u7684\u80fd\u91cf\u5bc6\u5ea6\uff0c\u800c\u4e14\u8fd8\u53ef\u4ee5\u5c06\u7535\u6781\u6750\u6599\u4ece\u539f\u5148\u7684\u542bLi\u9676\u74f7\u62d3\u5c55\u5230\u4e0d\u542bLi\u7684\u6750\u6599\uff0c\u5982\u6c27\u5316\u7269\u548c\u6c1f\u5316\u7269\u7b49\u3002\u57fa\u4e8eLi\u91d1\u5c5e\u8d1f\u6781\u7684\u4e0b\u4e00\u4ee3 Li\u91d1\u5c5e\u7535\u6c60\uff08LMB\uff09\uff0c\u5176\u6bd4\u5bb9\u91cf\u53ef\u4ee5\u8fbe\u5230\u4f20\u7edfLIBs\u76842~3\u500d\uff0c\u4f46\u7531\u4e8eLi\u91d1\u5c5e\u4e0e\u4f17\u591a\u6709\u673a\u7535\u89e3\u6db2\u7684\u80fd\u7ea7\u4e0d\u5339\u914d\uff0c\u6240\u4ee5\u4e8c\u8005\u5728\u70ed\u529b\u5b66\u4e0a\u662f\u4e0d\u7a33\u5b9a\u7684\uff0c\u4e14Li\u91d1\u5c5e\u6613\u4e8e\u548c\u7535\u89e3\u6db2\u6eb6\u5242\u53d1\u751f\u53cd\u5e94\u3002\u867d\u7136SEI\u819c\u7684\u5f62\u6210\u80fd\u591f\u5728\u4e00\u5b9a\u7a0b\u5ea6\u4e0a\u6291\u5236Li\u91d1\u5c5e\u4e0e\u6eb6\u5242\u53d1\u751f\u53cd\u5e94\uff0c\u4f46\u5927\u591a\u6570\u8fd9\u7c7b\u819c\u5e76\u4e0d\u80fd\u5bb9\u7eb3Li\u6c89\u79ef\u6240\u5f15\u8d77\u7684\u4e25\u91cd\u7684\u4f53\u79ef\u81a8\u80c0\uff0c\u6240\u4ee5Li\/\u7535\u89e3\u6db2\u754c\u9762\u7684\u4e0d\u7a33\u5b9a\u6027\u4f9d\u65e7\u6ca1\u80fd\u5f97\u5230\u5927\u5e45\u5ea6\u6539\u5584\uff0c\u4ece\u800c\u4e25\u91cd\u5236\u7ea6\u4e86Li\u91d1\u5c5e\u5728\u53ef\u5145\u7535\u7535\u6c60\u4e2d\u7684\u5e94\u7528\u3002<\/p>\n

\u3010\u6210\u679c\u7b80\u4ecb\u3011<\/strong><\/p>\n

\u8fd1\u65e5\uff0c \u4e2d\u79d1\u9662\u5b81\u6ce2\u6750\u6599\u6240\u738b\u5fb7\u5b87\u7814\u7a76\u5458\u3001\u4e0a\u6d77\u7845\u9178\u76d0\u7814\u7a76\u6240\u90ed\u5411\u6b23\u7814\u7a76\u5458<\/strong>\u8054\u5408\u7f8e\u56fd\u592a\u5e73\u6d0b\u897f\u5317\u56fd\u5bb6\u5b9e\u9a8c\u5ba4<\/strong>Ji-Guang (Jason) Zhang<\/strong>\u5728Nano Energy<\/em><\/strong>\u4e0a\u53d1\u8868\u4e86\u4e00\u7bc7\u9898\u4e3a\u201cStabilizing Li\/Electrolyte Interface with a Transplantable Protective Layer Based on Nanoscale LiF Domains<\/strong>\u201d\u7684\u6587\u7ae0\u3002\u5728\u8be5\u9879\u5de5\u4f5c\u4e2d\uff0c\u7814\u7a76\u4eba\u5458\u5f00\u53d1\u4e86\u4e00\u79cd\u53ef\u79fb\u690d\u6027\u5bccLiF\u5c42\uff08TLL\uff09\uff0c\u7528\u4ee5\u4fdd\u62a4Li\u91d1\u5c5e\u7535\u6781\u3002\u8be5TLL\u5c42\u7531\u4ea4\u8054\u7684\u7eb3\u7c73\u7ea7LiF\u57df\u6784\u6210\uff0c\u901a\u8fc7\u7535\u5316\u5b66\u8fd8\u539fNiF2<\/sub>\u7684\u65b9\u5f0f\u4eceCu\u57fa\u5e95\u4e0a\u5265\u79bb\u5f97\u5230\u3002\u8fd9\u79cd\u4eba\u5de5TLL\u819c\u53ef\u4ee5\u5c06\u65b0\u6c89\u6dc0\u7684\u91d1\u5c5eLi\u4e0e\u7535\u89e3\u6db2\u6eb6\u5242\u9694\u5f00\uff0c\u4ece\u800c\u907f\u514d\u63a5\u89e6\u53cd\u5e94\uff0c\u5927\u5e45\u5ea6\u63d0\u9ad8\u4e86Li\u91d1\u5c5e\u8d1f\u6781\u7684\u6027\u80fd\u3002\u6b64\u5916\uff0c\u8fd9\u79cd\u53ef\u79fb\u690d\u6027TLL\u819c\u8fd8\u80fd\u591f\u76f4\u63a5\u7528\u4f5c\u4f17\u591a\u7535\u6c60\u4f53\u7cfb\u7684\u72ec\u7acb\u4fdd\u62a4\u7ec4\u4ef6\uff0c\u5bf9\u7535\u6c60\u6027\u80fd\u7684\u63d0\u9ad8\u5177\u6709\u5f88\u597d\u7684\u4fc3\u8fdb\u4f5c\u7528\u3002<\/p>\n

\u3010\u56fe\u6587\u5bfc\u8bfb\u3011<\/strong><\/p>\n

\u56fe<\/strong>1\u00a0 TLL<\/strong>\u819c\u7684\u5f62\u8c8c\u8868\u5f81<\/strong><\/p>\n

\"\"<\/p>\n

(a)<\/strong> \u7535\u5316\u5b66\u8fd8\u539f\u8fc7\u7a0b\u4e2d\uff0cNiF2<\/sub>\u819c\u7ed3\u6784\u7684\u8f6c\u53d8\u53caTLL\u819c\u7684\u5f62\u6210\u793a\u610f\u56fe\uff1b<\/p>\n

(b-d) <\/strong>\u7535\u5316\u5b66\u8fd8\u539f\u524d\u540e\uff0cNiF2<\/sub>\u819c\u7684\u6570\u7801\u7167\u7247(b)\u3001SEM\u56fe\u50cf(c, d)\uff1b<\/p>\n

(e) <\/strong>TLL\u548cLiF\u7c89\u672b\u4e2dLiF\u76f8\u7684\u539f\u5b50\u95f4\u8dddd\u548c\u57df\u5c3a\u5bf8L\uff0c\u6570\u636e\u6765\u6e90\u4e8eLiF\u6676\u4f53\u7ed3\u6784(200)\u9762\u6240\u5728\u5cf0\u7684XRD\u5206\u6790\u3002<\/p>\n

\u56fe<\/strong>2\u00a0 HAADF-STEM<\/strong>\u53ca<\/strong>EDS<\/strong>\u8868\u5f81<\/strong><\/p>\n

\"\"<\/p>\n

(a, b) <\/strong>\u7535\u5316\u5b66\u8fd8\u539f\u524d\u540e\uff0cNiF2<\/sub>\u819c\u7684HAADF-STEM\u56fe\u50cf\u53ca\u5143\u7d20\u5206\u5e03\u56fe\uff1b<\/p>\n

(c) <\/strong>TLL\u819c\u7684HAADF-STEM\u653e\u5927\u56fe\u50cf\u53ca\u5143\u7d20\u5206\u5e03\u56fe\u3002<\/p>\n

\u56fe<\/strong>3 \u00a0\u7535\u5316\u5b66\u6027\u80fd\u6d4b\u8bd5<\/strong><\/p>\n

\"\"<\/p>\n

(a-e) <\/strong>Cu\/TLL\u7684SEM\u56fe\u50cf\uff1a\u521d\u59cb\u72b6\u6001\uff08a\uff09\u3001\u9996\u6b21Li\u91d1\u5c5e\u6c89\u79ef\uff08b\uff09\u3001\u9996\u6b21Li\u91d1\u5c5e\u6eb6\u51fa\uff08c\uff09\u3001\u7b2c\u4e8c\u6b21Li\u91d1\u5c5e\u6c89\u79ef\uff08d\uff09\u3001\u7b2c\u4e8c\u6b21\u91d1\u5c5eLi\u6eb6\u51fa\uff08e\uff09\uff1b<\/p>\n

(f) <\/strong>Cu\/TLL\u7535\u6781\u4e0a\uff0cLi\u9996\u6b21\u6c89\u79ef\/\u6eb6\u51fa\u7684\u5145\u653e\u7535\u66f2\u7ebf\uff1b<\/p>\n

(g) <\/strong>Li\u6c89\u79ef\u5728Li\u3001Cu\u3001Ni\u7b94\u4e0a\u7684\u653e\u7535\u66f2\u7ebf\uff1b<\/p>\n

(h) <\/strong>Li\u6c89\u79ef\u5728TLL\u819c\u548c\u4e00\u5c42LiF\u548cSuper-P\u7c89\u672b\u7ec4\u6210\u7684\u819c\u7684\u653e\u7535\u66f2\u7ebf\u3002<\/p>\n

\u56fe<\/strong>4\u00a0 TLL<\/strong>\u819c\u7684<\/strong>AFM<\/strong>\u8868\u5f81<\/strong><\/p>\n

\"\"<\/p>\n

\u4e0d\u540c\u63a2\u6d4b\u5c3a\u5ea6\u4e0b\uff0c<\/strong>TLL<\/strong>\u819c\u7684\u5f62\u8c8c\u548c\u76f8\u5e94\u7684<\/strong>QNM<\/strong>\u56fe\uff1a<\/strong><\/p>\n

(a) <\/strong>100 nm\uff1b<\/p>\n

(b) <\/strong>1 \u03bcm\u3002<\/p>\n

\u56fe<\/strong>5\u00a0 XPS<\/strong>\u8868\u5f81\u53ca\u9891\u7387\u963b\u6297\u8868\u5f81<\/strong><\/p>\n

\"\"<\/p>\n

(a, b) <\/strong>\u4e24\u6b21Li\u91d1\u5c5e\u6c89\u79ef\/\u6eb6\u51fa\u5faa\u73af\u540e\uff0c Cu\uff08a\uff09\u548cCu\/TLL\uff08b\uff09\u7535\u6781\u8868\u9762\u4e0d\u540c\u523b\u8680\u65f6\u95f4\u5bf9\u5e94\u7684Cu 2p XPS\u8c31\u56fe\uff1b<\/p>\n

(c) <\/strong>Cu\uff08c\uff09\u548cCu\/TLL\uff08d\uff09\u7535\u6781\u5728\u5145\u653e\u7535\u5faa\u73af\u8fc7\u7a0b\u4e2d\u7684\u963b\u6297\u6f14\u53d8\u53ca\u80fd\u594e\u65af\u7279\u56fe\uff0c\u5176\u4e2dRi<\/sub>\u548cRe<\/sub>\u5206\u522b\u8868\u793a\u754c\u9762\u963b\u6297\u548c\u7535\u89e3\u8d28\u963b\u6297\u3002<\/p>\n

\u56fe<\/strong>6\u00a0 <\/strong>\u5145\u653e\u7535\u6027\u80fd\u8868\u5f81<\/strong><\/p>\n

\"\"<\/p>\n

(a-c) <\/strong>TLL\u3001LiF\u591a\u5b54\u5c42\u3001NiO\u5c42\u57faCu-Li\u7535\u6c60\u7684\u5145\u653e\u7535\u66f2\u7ebf\uff1b<\/p>\n

(d) <\/strong>TLL\u3001LiF\u591a\u5b54\u5c42\u3001NiO\u5c42\u3001Cu\u57faCu-Li\u7535\u6c60\u7684\u5e93\u4f26\u6548\u7387\u66f2\u7ebf\uff0c\u5faa\u73af\u6d4b\u8bd5\u7684\u7535\u6d41\u5bc6\u5ea6\u548c\u5bb9\u91cf\u8d1f\u8377\u5206\u522b\u4e3a0.5 mA cm-2<\/sup>\u548c1 mAh cm-2<\/sup>\uff1b<\/p>\n

(e-g) <\/strong>\u5145\u653e\u7535\u5faa\u73af\u524d\u540e\uff0cTLL\u819c\uff08e\uff09\u3001LiF\u591a\u5b54\u819c\uff08f\uff09\u3001NiO\u819c\uff08g\uff09\u7684SEM\u56fe\u50cf\u3002<\/p>\n

\u56fe<\/strong>7\u00a0 <\/strong>\u6052\u6d41\u5faa\u73af\u6027\u80fd\u6d4b\u8bd5<\/strong><\/p>\n

\"\"<\/p>\n

\u5206\u522b\u4f7f\u7528Li\u91d1\u5c5e\u5355\u6781\u6216Li\/TLL\u590d\u5408\u7535\u6781\u7ec4\u88c5\u6210\u5bf9\u79f0\u7535\u6c60\u540e\uff0c\u5728\u4e0d\u540c\u56fa\u5b9a\u7535\u6d41\u5bc6\u5ea6\u53ca1mAh cm-2<\/sup>\u6c89\u79ef\/\u6eb6\u51fa\u5bb9\u91cf\u4e0b\uff0c\u6d4b\u8bd5\u5f97\u5230\u7684\u6052\u6d41\u5faa\u73af\u6027\u80fd\u56fe\uff1a\uff08a\uff090.5 mA cm-2<\/sup>\uff1b\uff08a\uff091 mA cm-2<\/sup>\uff1b\uff08a\uff092 mA cm-2<\/sup>\u3002<\/p>\n

\u56fe<\/strong>8\u00a0 TLL<\/strong>\u5728<\/strong>Li-LiFePO4<\/sub><\/strong>\u7535\u6c60\u4e2d\u7684\u5e94\u7528<\/strong><\/p>\n

\"\"<\/p>\n

(a, b) <\/strong>Li-LiFePO4<\/sub>\u7535\u6c60\uff08a\uff09\u53caLi\/TLL-LiFePO4<\/sub>\u7535\u6c60\uff08b\uff09\u7684\u5145\u653e\u7535\u66f2\u7ebf\uff1b<\/p>\n

(c, d) <\/strong>Li-LiFePO4<\/sub>\u7535\u6c60\u53caLi\/TLL-LiFePO4<\/sub>\u7535\u6c60\u7684\u5145\u653e\u7535\u5bb9\u91cf-\u5faa\u73af\u6d4b\u8bd5\u66f2\u7ebf\uff08c\uff09\u548c\u7535\u538b\u6ede\u540e-\u5faa\u73af\u66f2\u7ebf\uff0c\u5176\u4e2d\u5145\u653e\u7535\u500d\u7387\u4e3a0.5 C\/0.5 C\uff0c\u5bf9\u5e94\u7684\u7535\u6d41\u5bc6\u5ea6\u4e3a0.35 mA cm-2<\/sup>\/0.35 mA cm-2<\/sup>\uff1b<\/p>\n

(e) <\/strong>650\u4e2a\u5145\u653e\u7535\u5faa\u73af\u540eLi\u91d1\u5c5e\u7535\u6781\u548c1000\u4e2a\u5faa\u73af\u540eLi\/TLL\u7535\u6781\u7684\u6570\u7801\u7167\u7247\uff1b<\/p>\n

\u3010\u5c0f\u7ed3\u3011<\/strong><\/p>\n

\u5728\u672c\u6587\u4e2d\uff0c\u7814\u7a76\u4eba\u5458\u7814\u53d1\u4e86\u4e00\u79cd\u53ef\u79fb\u690d\u6027\u5bccLiF\u819c\uff08TLL\uff09\uff0c\u7528\u4ee5\u6539\u5584Li\u91d1\u5c5e\u8d1f\u6781\u7684\u5faa\u73af\u7a33\u5b9a\u6027\u80fd\u3002\u8fd9\u79cd\u7b80\u5355\u6613\u5f97\u7684\u4eba\u5de5TLL\u819c\u53ef\u4ee5\u4ece\u57fa\u5e95\u4e0a\u5265\u79bb\u800c\u6765\uff0c\u79fb\u690d\u5728\u5404\u79cd\u4e0d\u540c\u7684Li\u91d1\u5c5e\u7535\u6c60\u5f53\u4e2d\u3002\u5728Li-Cu\u7535\u6c60\u4e2d\uff0c\u4f7f\u7528TLL\u819c\u53ef\u4ee5\u663e\u8457\u63d0\u9ad8\u7535\u6c60\u7684\u5faa\u73af\u7a33\u5b9a\u6027\uff0c\u6bd4\u5355\u7eaf\u7684LI-Cu\u7535\u6c60\u591a\u7ecf\u8fc7300\u6b21\u5faa\u73af\u540e\uff0c\u4f7f\u7528TLL\u819c\u5c42\u7684\u7535\u6c60\u5e93\u4f26\u6548\u7387\u5927\u7ea6\u53ef\u4ee5\u4fdd\u6301\u572898%\u3002\u5728Li-LiFePO4<\/sub>\u7535\u6c60\u4f53\u7cfb\u4e2d\uff0c\u7ecf\u8fc7\u957f\u8fbe\u516d\u4e2a\u6708\u7684\u5145\u653e\u7535\u5faa\u73af\u6d4b\u8bd5\uff0c\u53731000\u6b21\u5faa\u73af\u540e\uff0c\u542b\u6709TLL\u4fdd\u62a4\u5c42\u7684\u7535\u6781\u4ecd\u7136\u53ef\u4ee5\u4fdd\u6301\u5176\u95ea\u4eae\u7684\u91d1\u5c5e\u8868\u9762\u3002\u5b9e\u9a8c\u7ed3\u679c\u8868\u660eTLL\u53ef\u4ee5\u6709\u6548\u5730\u7a33\u5b9aLi\/\u7535\u89e3\u6db2\u754c\u9762\uff0c\u4ece\u800c\u4f18\u5316Li\u91d1\u5c5e\u7535\u6c60\u4f53\u7cfb\u3002<\/p>\n

\u6587\u732e\u94fe\u63a5\uff1a<\/strong>Stabilizing Li\/Electrolyte Interface with a Transplantable Protective Layer Based on Nanoscale LiF Domains<\/a>(Nano Energy<\/em>, 2017, DOI: 10.1016\/j.nanoen.2017.07.052)<\/p>\n

\u672c\u6587\u7531\u6750\u6599\u4eba\u65b0\u80fd\u6e90\u7ec4 \u6df1\u6d77\u4e07\u91cc \u4f9b\u7a3f\uff0c\u6750\u6599\u725b\u7f16\u8f91\u6574\u7406\u3002<\/p>\n

\u6750\u6599\u725b\u7f51\u4e13\u6ce8\u4e8e\u8ddf\u8e2a\u6750\u6599\u9886\u57df\u79d1\u6280\u53ca\u884c\u4e1a\u8fdb\u5c55\uff0c\u8fd9\u91cc\u6c47\u96c6\u4e86\u5404\u5927\u9ad8\u6821\u7855\u535a\u751f\u3001\u4e00\u7ebf\u79d1\u7814\u4eba\u5458\u4ee5\u53ca\u884c\u4e1a\u4ece\u4e1a\u8005\uff0c\u5982\u679c\u60a8\u5bf9\u4e8e\u8ddf\u8e2a\u6750\u6599\u9886\u57df\u79d1\u6280\u8fdb\u5c55\uff0c\u89e3\u8bfb\u9ad8\u6c34\u5e73\u6587\u7ae0\u6216\u662f\u8bc4\u8ff0\u884c\u4e1a\u6709\u5174\u8da3\uff0c\u70b9\u6211\u52a0\u5165\u6750\u6599\u4eba\u7f16\u8f91\u90e8<\/a>\u3002<\/p>\n

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\u6750\u6599\u6d4b\u8bd5\uff0c\u6570\u636e\u5206\u6790\uff0c\u4e0a<\/strong>\u6d4b\u8bd5\u8c37<\/strong><\/a>\uff01<\/strong><\/p>\n","protected":false},"excerpt":{"rendered":"

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