{"id":95403,"date":"2017-08-11T06:30:01","date_gmt":"2017-08-10T22:30:01","guid":{"rendered":"http:\/\/www.cailiaoniu.com\/?p=95403"},"modified":"2017-08-10T23:20:51","modified_gmt":"2017-08-10T15:20:51","slug":"%e5%a4%a7%e8%bf%9e%e5%8c%96%e7%89%a9%e6%89%80nano-energy%ef%bc%9a%e5%b1%82%e9%97%b4%e8%b7%9d%e6%89%a9%e5%a4%a7%e7%9a%84%e7%a2%b1%e5%8c%96ti3c2-mxene%e7%ba%b3%e7%b1%b3%e5%b8%a6%e7%94%a8%e4%ba%8e","status":"publish","type":"post","link":"http:\/\/www.cailiaoniu.com\/?p=95403","title":{"rendered":"\u5927\u8fde\u5316\u7269\u6240Nano Energy\uff1a\u5c42\u95f4\u8ddd\u6269\u5927\u7684\u78b1\u5316Ti3C2 MXene\u7eb3\u7c73\u5e26\u7528\u4e8e\u9ad8\u5bb9\u91cf\u94a0\u79bb\u5b50\u548c\u94be\u79bb\u5b50\u7535\u6c60"},"content":{"rendered":"

\u3010\u5f15\u8a00\u3011<\/strong><\/p>\n

\u65e5\u76ca\u4e25\u5cfb\u7684\u80fd\u6e90\u95ee\u9898\u548c\u73af\u5883\u95ee\u9898\u5bf9\u7535\u5316\u5b66\u50a8\u80fd\u6280\u672f\u63d0\u51fa\u4e86\u65b0\u7684\u66f4\u5927\u7684\u6311\u6218\u3002\u4f5c\u4e3a\u76ee\u524d\u4e3b\u6d41\u7684\u53ef\u79fb\u52a8\u50a8\u80fd\u88c5\u7f6e\uff0c\u9502\u79bb\u5b50\u7535\u6c60(LIBs)\u5728\u8fd1\u5e74\u6765\u5f97\u5230\u8fc5\u901f\u7684\u53d1\u5c55\u3002\u7136\u800c\u76f8\u5bf9\u6709\u9650\u7684\u9502\u8d44\u6e90\u50a8\u91cf\uff0c\u76f8\u5bf9\u8f83\u9ad8\u7684\u6210\u672c\u4ee5\u53ca\u6f5c\u5728\u7684\u5b89\u5168\u95ee\u9898\u5728\u4e00\u5b9a\u7a0b\u5ea6\u4e0a\u9650\u5236\u4e86\u9502\u79bb\u5b50\u7535\u6c60\u7684\u5168\u9762\u666e\u53ca\u3002\u4e3a\u4e86\u89e3\u51b3LIBs\u5b58\u5728\u7684\u4e00\u7cfb\u5217\u95ee\u9898\uff0c\u7814\u7a76\u4eba\u5458\u63d0\u51fa\u4e86\u4f7f\u7528\u94a0\u79bb\u5b50\u7535\u6c60(SIBs)\u7b49\u975e\u9502\u79bb\u5b50\u7535\u6c60\u66ff\u4ee3LIBs\u7684\u89e3\u51b3\u65b9\u6848\u3002SIBs\u5177\u5907\u50a8\u91cf\u4e30\u5bcc\u3001\u6210\u672c\u4f4e\u5ec9\u3001\u6c27\u5316\u8fd8\u539f\u7535\u52bf\u5408\u9002(E0 <\/sup>Na+<\/sup>\/Na = 2.71 V vs SHE)\u3001\u80fd\u91cf\u5bc6\u5ea6\u4e0eLIBs\u76f8\u8fd1\u7b49\u7279\u70b9\uff0c\u6210\u4e3a\u66ff\u4ee3LIBs\u7406\u60f3\u7684\u7535\u5316\u5b66\u50a8\u80fd\u88c5\u7f6e\u3002\u94a0\u79bb\u5b50\u7535\u6c60(SIBs)\u548c\u94be\u79bb\u5b50\u7535\u6c60(PIBs)\u76ee\u524d\u5b58\u5728\u7684\u4e3b\u8981\u95ee\u9898\u662f\u7f3a\u5c11\u5408\u9002\u7684\u7535\u89e3\u8d28\u548c\u7535\u6781\u6750\u6599\uff0c\u56e0\u6b64\u5f00\u53d1\u51fa\u9ad8\u6027\u80fd\u7684\u7535\u6781\u6750\u6599\u6210\u4e3a\u63a8\u52a8\u975e\u9502\u79bb\u5b50\u7535\u6c60\u53d1\u5c55\u7684\u4e00\u9879\u7d27\u8feb\u7684\u4efb\u52a1\u3002<\/p>\n

MXene\u7531\u4e8e\u72ec\u7279\u7684\u5fae\u89c2\u5f62\u8c8c\u3001\u8f83\u9ad8\u7684\u7406\u8bba\u5bb9\u91cf\u4ee5\u53ca\u53ef\u8c03\u7684\u5c42\u95f4\u8ddd\uff0c\u6210\u4e3a\u91d1\u5c5e\u79bb\u5b50\u7535\u6c60(LIBs, SIBs, PIBs)\u7406\u60f3\u7684\u7535\u6781\u6750\u6599\u3002Ti3<\/sub>C2<\/sub> MXene \u7eb3\u7c73\u7247(Ti3<\/sub>C2 <\/sub>MNSs)\u53ca\u5176\u884d\u751f\u7269\u5177\u5907\u4f18\u5f02\u7684\u7535\u5316\u5b66\u6027\u80fd\uff0c\u6210\u4e3a\u76ee\u524d\u7814\u7a76\u7684\u70ed\u70b9\u3002\u7814\u7a76\u53d1\u73b0\uff1a\u7531\u4e8e\u72ec\u7279\u7684\u591a\u5c42Li\u5438\u9644\u7279\u6027\u4ee5\u53ca\u8f83\u4f4e\u7684Li\u539f\u5b50\u6269\u6563\u52bf\u5792\uff0cTi3<\/sub>C2<\/sub> MXene\u7eb3\u7c73\u7247\u7528\u4f5cLIBs\u8d1f\u6781\u6750\u6599\u65f6\uff0c\u53ef\u9006\u5bb9\u91cf\u4ecb\u4e8e320-410 mAh\/g\uff0c\u4e14\u500d\u7387\u6027\u80fd\u7531\u4e8e\u77f3\u58a8\u7535\u6781\u3002\u5f53Ti3<\/sub>C2 <\/sub>MNSs\u7528\u4e8e\u8d85\u7ea7\u7535\u5bb9\u5668\u65f6\uff0c\u4f53\u79ef\u7535\u5bb9\u7ea6\u4e3a300-900 F\/cm3<\/sup>\u3002\u8fd1\u671f\u7684\u7406\u8bba\u7814\u7a76\u548c\u5b9e\u9a8c\u6d4b\u8bd5\u8868\u660e\uff1aTi3<\/sub>C2 <\/sub>MNSs \u5177\u5907\u8f83\u9ad8\u7684\u500d\u7387\u5bb9\u91cf\u548c\u8f83\u597d\u7684\u957f\u671f\u5faa\u73af\u7a33\u5b9a\u6027\uff0c\u9002\u5408\u6700\u4e3a\u94a0\u79bb\u5b50\u7535\u6c60(SIBs)\u548c\u94be\u79bb\u5b50\u7535\u6c60(PIBs)\u7684\u7535\u6781\u6750\u6599\u3002MXene\u4fd8\u83b7\u7684Na+<\/sup>\u7684\u652f\u67f1\u6548\u5e94(pillaring effect)\u53ef\u4ee5\u6709\u6548\u4fdd\u6301\u5c42\u95f4\u8ddd\u7684\u7a33\u5b9a\uff0c\u6709\u5229\u4e8e\u5b9e\u73b0\u5feb\u901f\u7684\u53ef\u9006\u94a0\u5316-\u53bb\u94a0\u5316\u8fc7\u7a0b\u3002<\/p>\n

\u3010\u6210\u679c\u7b80\u4ecb\u3011<\/strong><\/p>\n

\u8fd1\u65e5\uff0c\u4e2d\u79d1\u9662\u5927\u8fde\u5316\u7269\u6240\u7684\u5434\u5fe0\u5e05<\/strong>(<\/strong>\u901a\u8baf\u4f5c\u8005<\/strong>)<\/strong>\u7b49<\/strong>\u5728Nano Energy<\/strong>\u53d1\u8868\u4e86\u9898\u4e3a\u201cAlkalized Ti3<\/sub>C2<\/sub> MXene Nanoribbons with Expanded Interlayer Spacing for High-Capacity Sodium and Potassium Ion Batteries<\/strong>\u201d \u7684\u7814\u7a76\u8bba\u6587\uff0c\u62a5\u9053\u4e86\u78b1\u5316\u5904\u7406\u7684Ti3<\/sub>C2 <\/sub>MXene\u7eb3\u7c73\u5e26\u7528\u4e8e\u94a0\u79bb\u5b50\u7535\u6c60\u548c\u94be\u79bb\u5b50\u7535\u6c60\u7684\u6700\u65b0\u7814\u7a76\u6210\u679c\u3002\u7814\u7a76\u56e2\u961f\u9996\u5148\u91c7\u7528\u56fa-\u6db2\u53cd\u5e94\u6cd5\u5236\u5907\u5f97\u5e26Ti3<\/sub>AlC2<\/sub>\u524d\u9a71\u4f53\uff0c\u7136\u540e\u5bf9\u524d\u9a71\u4f53\u8fdb\u884c\u6c22\u6c1f\u9178(HF, 40 wt%)\u5904\u7406\u5f97\u5230Ti3<\/sub>C2<\/sub> MXene \u7eb3\u7c73\u7247(Ti3<\/sub>C2 <\/sub>MNSs)\u4e2d\u95f4\u4f53\uff0c\u6700\u540e\u5728\u5e38\u6e29\u4e0b\u5c06Ti3<\/sub>C2 <\/sub>MNSs \u5728KOH\u6eb6\u6db2\u4e2d\u9707\u8361\u5904\u7406\u5f97\u5230\u5c42\u95f4\u8ddd\u6269\u5927\u7684\u78b1\u5316Ti3<\/sub>C2 <\/sub>MXene\u7eb3\u7c73\u5e26(a-Ti3<\/sub>C2 <\/sub>MNRs)\u3002\u7814\u7a76\u53d1\u73b0\uff1aa-Ti3<\/sub>C2 <\/sub>MNRs\u7684\u79bb\u5b50\u53cd\u5e94\u52a8\u529b\u5b66\u548c\u7ed3\u6784\u7a33\u5b9a\u6027\u90fd\u5f97\u5230\u4e86\u660e\u663e\u7684\u6539\u5584\u3002\u7528\u4f5c\u94a0\u79bb\u5b50\u7535\u6c60(SIBs)\u548c\u94be\u79bb\u5b50\u7535\u6c60(PIBs)\u8d1f\u6781\u6750\u6599\u65f6\uff0ca-Ti3<\/sub>C2 <\/sub>MNRs\u8868\u73b0\u51fa\u4f18\u5f02\u7684\u7535\u5316\u5b66\u6027\u80fd\uff1a\u5f53\u7535\u6d41\u5bc6\u5ea6\u4e3a20 mA\/g\u65f6\uff0cSIBs\u548cPIBs\u7684\u53ef\u9006\u5bb9\u91cf\u5206\u522b\u4e3a168 mAh\/g\u548c136 mAh\/g\uff1b\u5f53\u7535\u6d41\u5bc6\u5ea6\u589e\u5927\u81f3200 mA\/g\u65f6\uff0cSIBs\u548cPIBs\u7684\u53ef\u9006\u5bb9\u91cf\u5206\u522b\u4e3a84 mAh\/g\u548c78 mAh\/g\uff1b\u4f7f\u7528a-Ti3<\/sub>C2 <\/sub>MNRs\u7535\u6781\u6750\u6599\u7684SIBs\u548cPIBs\u7684\u7a33\u5b9a\u6027\u4e5f\u8f83\u4e3a\u51fa\u8272\uff1a\u5728200 mA\/g\u7684\u9ad8\u7535\u6d41\u5bc6\u5ea6\u4e0b\u5faa\u73af500\u5708\u540e\u4ecd\u53ef\u5206\u522b\u4fdd\u755950 mAh\/g\u548c42 mAh\/g\u7684\u53ef\u9006\u5bb9\u91cf\uff0c\u7531\u4e8e\u76ee\u524d\u62a5\u9053\u7684\u7edd\u5927\u591a\u6570MXene\u7535\u6781\u6750\u6599\u3002\u8be5\u78b1\u5316\u65b9\u6cd5\u6709\u671b\u63a8\u5e7f\u81f3\u5176\u4ed6\u4e09\u7ef4MXene\u7ed3\u6784\u7684\u6784\u5efa\uff0c\u5e76\u62d3\u5bbdMXene\u7c7b\u6750\u6599\u7684\u5e94\u7528\u8303\u56f4\u3002<\/p>\n

\u3010\u56fe\u6587\u5bfc\u8bfb\u3011<\/strong><\/p>\n

\u56fe<\/strong>1 a-Ti3<\/sub>C2 <\/sub>MNRs <\/strong>\u7684\u5236\u5907<\/strong><\/p>\n

\"\"<\/p>\n

\uff08a\uff09a-Ti3<\/sub>C2 <\/sub>MNRs \u7684\u5408\u6210\u793a\u610f\u56fe\u3002\u9996\u5148\u5408\u6210Ti3<\/sub>AlC2<\/sub> MAX\u76f8\uff1b\u7136\u540e\u752840 % HF\u5265\u79bbAl\u5c42\uff0c\u5f97\u5230Ti3<\/sub>C2<\/sub> MNSs\uff1b\u6700\u540eKOH\u6eb6\u6db2\u9707\u8361\u5904\u7406\u5f97\u5230a-Ti3<\/sub>C2<\/sub> MNRs\u3002<\/p>\n

(b-d) \u4f4e\u653e\u5927\u500d\u6570SEM\u56fe\u7247: (b) Ti3<\/sub>AlC2<\/sub>, (c) Ti3<\/sub>C2<\/sub> MNSs, (d) a-Ti3<\/sub>C2<\/sub> MNRs\u3002<\/p>\n

\u56fe<\/strong>2 a-Ti3<\/sub>C2<\/sub> MNRs<\/strong>\u7684\u76f8\u8c8c\u8868\u5f81<\/strong><\/p>\n

\"\"<\/p>\n

(a) a-Ti3<\/sub>C2<\/sub> MNRs\u7684\u4f4e\u500dSEM\u56fe\u7247\u3002<\/p>\n

(b) a-Ti3<\/sub>C2<\/sub> MNRs\u7684\u9ad8\u500dSEM\u56fe\u7247\u3002<\/p>\n

(c) a-Ti3<\/sub>C2<\/sub> MNRs\u7684TEM\u56fe\u7247\u3002<\/p>\n

(d-f) a-Ti3<\/sub>C2<\/sub> MNRs\u7684\u9ad8\u5206\u8fa8TEM\u56fe\u7247\uff1a(b) \u5bbd\u5ea6\u4e3a8 nm\u7684\u5355\u6839MNR\uff0c\u5bf9\u5e94(c)\u4e2d\u7684\u4f4d\u7f6eA\uff1b(e) \u5bbd\u5ea6\u4e3a16 nm\u7684\u81ea\u7f20\u7ed5MNR\uff0c\u5bf9\u5e94(c)\u4e2d\u7684\u4f4d\u7f6eB\uff1b(f) \u5bbd\u5ea6\u4e3a22 nm\u7684\u5e73\u5766MNR\u3002<\/p>\n

(g-k) a-Ti3<\/sub>C2<\/sub> MNRs\u7684EDX\u5143\u7d20\u5206\u5e03\u56fe\u7247\uff1a(g) Ti\u5143\u7d20; (h) C\u5143\u7d20; (i) K\u5143\u7d20; (j) O\u5143\u7d20; (k) F\u5143\u7d20\u3002<\/p>\n

\u56fe<\/strong>3 a-Ti3<\/sub>C2<\/sub> MNRs<\/strong>\uff0c<\/strong>Ti3<\/sub>C2<\/sub> MNSs<\/strong>\u548c<\/strong>Ti3<\/sub>AlC2<\/sub><\/strong>\u7684\u7ed3\u6784\u8868\u5f81<\/strong><\/p>\n

\"\"<\/p>\n

(a) a-Ti3<\/sub>C2<\/sub>\uff0cTi3<\/sub>C2<\/sub>\u548c Ti3<\/sub>AlC2<\/sub>\u7684XRD\u7279\u5f81\u884d\u5c04\u8c31\u56fe\u3002<\/p>\n

(b) C1s\u548cK2p\u7684XPS\u8c31\u56fe\u3002<\/p>\n

(c) a-Ti3<\/sub>C2<\/sub>\uff0cTi3<\/sub>C2<\/sub>\u548c Ti3<\/sub>AlC2<\/sub>\u7684O1s XPS\u8c31\u56fe\u3002<\/p>\n

(d) a-Ti3<\/sub>C2<\/sub>\uff0cTi3<\/sub>C2<\/sub>\u548c Ti3<\/sub>AlC2<\/sub>\u7684\u6c2e\u5438\u9644\u7b49\u6e29\u7ebf\u3002<\/p>\n

\u56fe<\/strong>4. a-Ti3<\/sub>C2<\/sub> MNRs<\/strong>\u7528\u4e8e<\/strong>SIBs<\/strong>\u65f6\u7684\u7535\u5316\u5b66\u8868\u5f81<\/strong><\/p>\n

\"\"<\/p>\n

(a) \u5faa\u73af\u4f0f\u5b89\u66f2\u7ebf \u626b\u63cf\u533a\u95f4\uff1a0.01-3.0 V\uff1b\u626b\u63cf\u901f\u7387\uff1a0.1 mV\/s\u3002<\/p>\n

(b) \u4e0d\u540c\u7535\u6d41\u5bc6\u5ea6\u4e0b\u7684\u6052\u6d41\u5145\u653e\u7535\u66f2\u7ebf\uff1a\u7535\u6d41\u5bc6\u5ea6\u533a\u95f4\uff1a20-300 mA\/g\u3002<\/p>\n

(c) a-Ti3<\/sub>C2<\/sub> MNRs\u7684\u500d\u7387\u6027\u80fd\u3002<\/p>\n

(d) a-Ti3<\/sub>C2<\/sub> MNRs \u5728\u7535\u6d41\u5bc6\u5ea6\u4e3a200 mA\/g\u7684\u957f\u671f\u5faa\u73af\u6027\u80fd\u548c\u5e93\u4f26\u6548\u7387\u66f2\u7ebf\u3002<\/p>\n

\u56fe<\/strong>5. a-Ti3<\/sub>C2<\/sub> MNRs<\/strong>\u7528\u4e8e<\/strong>PIBs<\/strong>\u65f6\u7684\u7535\u5316\u5b66\u8868\u5f81<\/strong><\/p>\n

\"\"<\/p>\n

(a) \u5faa\u73af\u4f0f\u5b89\u66f2\u7ebf \u626b\u63cf\u533a\u95f4\uff1a0.01-3.0 V\uff1b\u626b\u63cf\u901f\u7387\uff1a0.1 mV\/s\u3002<\/p>\n

(b) \u4e0d\u540c\u7535\u6d41\u5bc6\u5ea6\u4e0b\u7684\u6052\u6d41\u5145\u653e\u7535\u66f2\u7ebf\uff1a\u7535\u6d41\u5bc6\u5ea6\u533a\u95f4\uff1a20-300 mA\/g\u3002<\/p>\n

(c) a-Ti3<\/sub>C2<\/sub> MNRs\u7684\u500d\u7387\u6027\u80fd\u3002<\/p>\n

(d) a-Ti3<\/sub>C2<\/sub> MNRs \u5728\u7535\u6d41\u5bc6\u5ea6\u4e3a200 mA\/g\u7684\u957f\u671f\u5faa\u73af\u6027\u80fd\u548c\u5e93\u4f26\u6548\u7387\u66f2\u7ebf\u3002<\/p>\n

\u3010\u5c0f\u7ed3\u3011<\/strong><\/p>\n

\u672c\u6587\u901a\u8fc7KOH\u6eb6\u6db2\u5bf9Ti3<\/sub>C2<\/sub> MXene\u7eb3\u7c73\u7247\u8fdb\u884c\u78b1\u5316\u5904\u7406\u5f97\u5230\u4e86\u5c42\u95f4\u8ddd\u6269\u5927\u7684\u78b1\u5316Ti3<\/sub>C2<\/sub> MXene\u7eb3\u7c73\u5e26\uff0c\u5e76\u5c06\u5176\u6210\u529f\u5e94\u7528\u4e8e\u94a0\u79bb\u5b50\u7535\u6c60(SIBs)\u548c\u94be\u79bb\u5b50\u7535\u6c60(PIBs)\u3002\u7531\u4e8e\u5c42\u95f4\u8ddd\u7684\u6269\u5927\u548c\u4e09\u7ef4\u591a\u5b54\u7ed3\u6784\u7684\u5b58\u5728\uff0ca-Ti3<\/sub>C2<\/sub> MNRs\u8868\u73b0\u51fa\u4f18\u5f02\u7684\u7535\u5316\u5b66\u6027\u80fd\u548c\u5faa\u73af\u7a33\u5b9a\u6027\u3002\u8be5\u78b1\u5316\u65b9\u6cd5\u6709\u671b\u63a8\u5e7f\u81f3\u5176\u5b83\u4e09\u7ef4MXene\u7ed3\u6784\u7684\u6784\u5efa\uff0c\u5e76\u8fdb\u4e00\u6b65\u62d3\u5bbdMXene\u7c7b\u6750\u6599\u7684\u5e94\u7528\u8303\u56f4\u3002<\/p>\n

\u6587\u732e\u94fe\u63a5<\/strong>\uff1aAlkalized Ti3<\/sub>C2<\/sub> MXene Nanoribbons with Expanded Interlayer Spacing for High-Capacity Sodium and Potassium Ion Batteries<\/a>(Nano Energy, 2017, DOI: 10.1016\/j.nanoen.2017.08.002)<\/p>\n

\u672c\u6587\u7531\u6750\u6599\u4eba\u7f16\u8f91\u90e8\u5f20\u6770\u7f16\u8bd1\uff0c\u9ec4\u8d85\u5ba1\u6838\uff0c\u70b9\u6211\u52a0\u5165\u6750\u6599\u4eba\u7f16\u8f91\u90e8<\/a>\u3002<\/u><\/p>\n

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