{"id":95794,"date":"2017-08-12T06:30:03","date_gmt":"2017-08-11T22:30:03","guid":{"rendered":"http:\/\/www.cailiaoniu.com\/?p=95794"},"modified":"2017-08-11T16:45:12","modified_gmt":"2017-08-11T08:45:12","slug":"%e6%b5%8e%e5%8d%97%e5%a4%a7%e5%ad%a6%ef%bc%9aadv-energy-mater-%ef%bc%9a%e8%b6%85%e8%96%84%e5%a4%9a%e5%ad%94%e4%b8%89%e7%bb%b4%e7%ba%b3%e7%b1%b3%e7%89%87%e7%bd%91%e7%bb%9c%e7%9a%84%e8%b6%85%e9%ab%98","status":"publish","type":"post","link":"http:\/\/www.cailiaoniu.com\/?p=95794","title":{"rendered":"\u6d4e\u5357\u5927\u5b66Adv. Energy Mater.\uff1a\u8d85\u8584\u591a\u5b54\u4e09\u7ef4\u7eb3\u7c73\u7247\u7f51\u7edc\u7684\u8d85\u9ad8\u80fd\u91cf\u5bc6\u5ea6\u975e\u5bf9\u79f0\u7535\u5bb9\u5668\u6b63\u6781"},"content":{"rendered":"

\u3010<\/strong>\u5f15\u8a00<\/strong>\u3011<\/strong><\/p>\n

\u968f\u7740\u4fbf\u643a\u5f0f\u7535\u5b50\u8bbe\u5907\u9700\u6c42\u7684\u5feb\u901f\u589e\u957f\uff0c\u517c\u5177\u9ad8\u529f\u7387\u3001\u5feb\u901f\u5145\u653e\u7535\u3001\u957f\u5bff\u547d\u3001\u73af\u5883\u53cb\u597d\u7b49\u7279\u6027\u7684\u975e\u5bf9\u79f0\u8d85\u7ea7\u7535\u5bb9\u5668\u5f97\u5230\u4e86\u7814\u7a76\u4eba\u5458\u7684\u5e7f\u6cdb\u5173\u6ce8\u3002\u5bf9\u4e8e\u8d85\u7ea7\u7535\u5bb9\u5668\u7684\u7814\u7a76\u6709\u4e24\u4e2a\u91cd\u8981\u7684\u7814\u7a76\u65b9\u5411\uff1a\u4e00\u662f\u63d0\u9ad8\u5668\u4ef6\u7684\u50a8\u80fd\u5bc6\u5ea6\u548c\u5faa\u73af\u7a33\u5b9a\u6027\uff0c\u4e8c\u662f\u6700\u5927\u9650\u5ea6\u7684\u589e\u5f3a\u5668\u4ef6\u673a\u68b0\u6027\u80fd\u3002\u901a\u8fc7\u63d0\u9ad8\u7535\u6781\u6750\u6599\u7684\u6bd4\u7535\u5bb9\u3001\u8bbe\u8ba1\u975e\u5bf9\u79f0\u578b\u8d85\u7ea7\u7535\u5bb9\u5668\uff08\u62d3\u5bbd\u5668\u4ef6\u5de5\u4f5c\u7535\u538b\uff09\uff0c\u90fd\u80fd\u591f\u660e\u663e\u7684\u63d0\u9ad8\u8d85\u7ea7\u7535\u5bb9\u5668\u7684\u50a8\u80fd\u5bc6\u5ea6\uff1b\u800c\u5668\u4ef6\u7684\u673a\u68b0\u6027\u80fd\u7684\u6539\u5584\u5219\u9700\u8981\u4f18\u5316\u7535\u6781\u7ed3\u6784\u548c\u5668\u4ef6\u7ed3\u6784\u3002\u5236\u5907\u4e09\u7ef4\u9635\u5217\u7ed3\u6784\u6765\u589e\u52a0\u6d3b\u6027\u6750\u6599\u4e0e\u7535\u89e3\u6db2\u63a5\u89e6\u7684\u6d3b\u6027\u4f4d\u70b9\uff0c\u53ef\u4ee5\u6709\u6548\u7684\u63d0\u9ad8\u7535\u6781\u6750\u6599\u7684\u7535\u5316\u5b66\u6027\u80fd\u3002\u901a\u8fc7\u5236\u5907\u81ea\u652f\u6491\u7535\u6781\/\u9009\u53d6\u5bfc\u7535\u6027\u826f\u597d\u7684\u57fa\u5e95\u53ef\u4ee5\u6709\u6548\u7684\u89e3\u51b3\u5668\u4ef6\u7684\u673a\u68b0\u6027\u80fd\u95ee\u9898\u3002<\/p>\n

\u4f5c\u4e3a\u8d85\u7ea7\u7535\u5bb9\u5668\u7684\u91cd\u8981\u7ec4\u6210\u90e8\u5206\uff0c\u5728\u4f17\u591a\u7684\u7535\u6781\u6750\u6599\u4e2d\u53cc\u91d1\u5c5e\u786b\u5316\u7269\u4e0e\u76f8\u5e94\u7684\u5355\u91d1\u5c5e\u786b\u5316\u7269\u76f8\u6bd4\u62e5\u6709\u4e30\u5bcc\u7684\u6c27\u5316\u8fd8\u539f\u53cd\u5e94\u6d3b\u6027\u4f4d\u70b9\uff1b\u76f8\u6bd4\u4e8e\u76f8\u5e94\u7684\u91d1\u5c5e\u6c27\u5316\u7269\u5177\u6709\u66f4\u9ad8\u7684\u5bfc\u7535\u6027\u548c\u7535\u5316\u5b66\u6d3b\u6027\u3002\u5408\u7406\u7684\u8bbe\u8ba1\u7eb3\u7c73\u7ed3\u6784\u80fd\u591f\u6709\u6548\u7684\u63d0\u9ad8\u6750\u6599\u672c\u8eab\u7684\u5bfc\u7535\u6027\u548c\u5229\u7528\u7387\uff0c\u5176\u4e2d2D\u7eb3\u7c73\u6750\u6599\u7531\u4e8e\u5404\u5411\u5f02\u6027\u7ed3\u6784\u548c\u9ad8\u7684\u8868\u9762\u4f53\u79ef\u6bd4\u6709\u6548\u7684\u63d0\u9ad8\u4e86\u6750\u6599\u7684\u5316\u5b66\u53cd\u5e94\u754c\u9762\u548c\u7f29\u77ed\u4e86\u79bb\u5b50\u4f20\u8f93\u8ddd\u79bb\u3002<\/p>\n

\u3010<\/strong>\u6210<\/strong>\u679c\u7b80\u4ecb<\/strong>\u3011<\/strong><\/p>\n

\u6d4e\u5357\u5927\u5b66\u5f90\u9521\u91d1\u6559\u6388\uff08\u901a\u8baf\u4f5c\u8005\uff09\u4e0e\u534e\u4e2d\u79d1\u6280\u5927\u5b66\u7fdf\u5929\u4f51\u6559\u6388\u548c\u674e\u4f1a\u5de7\u6559\u6388\uff08\u901a\u8baf\u4f5c\u8005\uff09\u5408\u4f5c\u5728Adv. Energy Mater.\u5728\u7ebf\u53d1\u8868\u9898\u4e3a\u201cUltrathin and Porous Ni3<\/sub>S2<\/sub>\/CoNi2<\/sub>S4<\/sub>3D-Network Structure for Superhigh Energy Density Asymmetric Supercapacitors\u201d\u7684\u6587\u7ae0\u3002\u8be5\u8bfe\u9898\u7ec4\u91c7\u7528\u4e24\u6b65\u6cd5\u5236\u5907Ni3<\/sub>S2<\/sub>\/CoNi2<\/sub>S4<\/sub>\uff1a\u7b2c\u4e00\u6b65\u5236\u5907NiCo-\u524d\u9a71\u4f53\u7eb3\u7c73\u7247\u9635\u5217\uff1b\u7b2c\u4e8c\u6b65NiCo-\u524d\u9a71\u4f53\u7eb3\u7c73\u7247\u9635\u5217\u786b\u5316\u4e3aNi3<\/sub>S2<\/sub>\/CoNi2<\/sub>S4<\/sub>\u4e09\u7ef4\u7eb3\u7c73\u7247\u7f51\u7edc\u3002\u7814\u7a76\u53d1\u73b0\u4ee5Na2<\/sub>S.9H2<\/sub>O\u4e3a\u786b\u6e90\u9009\u7528\u5408\u9002\u7684\u786b\u5316\u65f6\u95f4\u548c\u6e29\u5ea6\uff0c\u53ef\u4ee5\u5408\u6210\u7eb3\u7c73\u9897\u7c92\u5747\u5300\u5206\u5e03\u5728\u7eb3\u7c73\u7247\u4e0a\u7684Ni3<\/sub>S2<\/sub>\u548cCoNi2<\/sub>S4<\/sub>\u5171\u5b58\u7684\u7f51\u72b6\u7ed3\u6784\uff0c\u8fd9\u79cd\u7ed3\u6784\u5177\u6709\u8d85\u4e30\u5bcc\u7684\u8fb9\u7f18\u6d3b\u6027\u4f4d\u70b9\uff0c\u6709\u6548\u7684\u589e\u52a0\u4e86\u7eb3\u7c73\u7247\u4e0e\u7535\u89e3\u6db2\u7684\u6709\u6548\u63a5\u89e6\u9762\u3002\u6b64\u5de5\u4f5c\u8fd8\u9a8c\u8bc1\u4e86\u4e24\u6b65\u786b\u5316\u6cd5\u53ef\u4ee5\u5f88\u597d\u7684\u4fdd\u6301\u524d\u9a71\u4f53\u7684\u539f\u6709\u5f62\u8c8c\uff0c\u800c\u4e14\u6b64\u79cd\u786b\u5316\u6cd5\u53ef\u4ee5\u7c97\u5316\u7eb3\u7c73\u7247\u7684\u8868\u9762\u3002\u4f46\u662f\u7ecf\u8fc7\u9ad8\u6e29\u9000\u706b\u4f1a\u4f7f\u7eb3\u7c73\u7247\u7684\u7ed3\u6784\u53d1\u751f\u660e\u663e\u7684\u7ed3\u6784\u584c\u9677\u5e76\u4e14\u7247\u7ed3\u6784\u6709\u53d8\u8584\u7684\u8d8b\u52bf\u3002Ni3<\/sub>S2<\/sub>\/CoNi2<\/sub>S4<\/sub>\/NF\u4e09\u7ef4\u7eb3\u7c73\u7247\u7f51\u72b6\u7ed3\u6784\u5177\u6709\u9ad8\u7684\u6bd4\u7535\u5bb9(2435 F g\u22121<\/sup>\u5728\u7535\u6d41\u5bc6\u5ea6\u4e3a2 A g\u2212<\/sup>1<\/sup>\u65f6)\u548c\u6781\u9ad8\u7535\u5bb9\u4fdd\u6301\u738780 % (1940F g\u2212<\/sup>1<\/sup>\u5728\u7535\u6d41\u5bc6\u5ea6\u4e3a20A g\u2212<\/sup>1<\/sup>)\u4ee5\u53ca\u826f\u597d\u7684\u7535\u5316\u5b66\u5bfc\u7535\u6027.\u00a0\u5e76\u8fdb\u4e00\u6b65\u4ee5Ni3<\/sub>S2<\/sub>\/CoNi2<\/sub>S4<\/sub>\/NF\u4e3a\u8d85\u7ea7\u7535\u5bb9\u5668\u7684\u6b63\u6781\u6750\u6599\uff0c\u4ee5\u8d85\u7ea7\u7535\u5bb9\u6d3b\u6027\u70ad(AC)\u4e3a\u8d1f\u6781\u6750\u6599\u7ec4\u88c5\u6210\u975e\u5bf9\u79f0\u7535\u5bb9\u5668\uff0c\u62e5\u6709\u6770\u51fa\u7684\u6bd4\u7535\u5bb9(175 F g-1<\/sup>\u57281 A g-1<\/sup>)\u7a33\u5b9a\u6027\uff0c\u673a\u68b0\u6027\uff0c\u5bbd\u7684\u7535\u538b\u7a97\u53e3(1.7 V)\u548c\u9ad8\u7684\u80fd\u91cf\u5bc6\u5ea6(50.7 W h kg\u2212<\/sup>1<\/sup>\u5728\u529f\u7387\u5bc6\u5ea6\u4e3a1594.1\u00a0 W kg\u2212<\/sup>1<\/sup>\uff1b40.0 W h kg\u2212<\/sup>1<\/sup>\u5728\u529f\u7387\u5bc6\u5ea6\u4e3a17349.4 W kg\u2212<\/sup>1<\/sup>)\u3002<\/p>\n

\u3010<\/strong>\u56fe<\/strong>\u6587\u5bfc\u8bfb<\/strong>\u3011<\/strong><\/p>\n

\u56fe\u4e00\uff1a\u8d85\u7ea7\u7535\u5bb9\u5668\u7535\u6781\u5408\u6210\u53ca\u5176\u50a8\u80fd\u793a\u610f\u56fe<\/strong><\/p>\n

\"\"<\/p>\n

\u56fe\u4e8c\uff1aSEM\u5f62\u8c8c\u8868\u5f81\u548c\u7ed3\u6784\u5206\u6790<\/strong><\/p>\n

\"\"<\/p>\n

(a) (b) \u548c(c)NiCo-\u524d\u9a71\u4f53\u4f4e\u500d\u548c\u9ad8\u500d\u626b\u63cf\u56fe(SEM), (c-1)\u524d\u9a71\u4f53\u7eb3\u7c73\u7247\u7684\u7ed3\u6784\u6a21\u578b\u3002<\/p>\n

(d) (e)\u548c(f)Ni3<\/sub>S2<\/sub>\/CoNi2<\/sub>S4<\/sub>\u4e09\u7ef4\u7eb3\u7c73\u7247\u7f51\u7edc\u7684\u4f4e\u500d\u548c\u9ad8\u500d\u626b\u63cf\u56fe(SEM),(f-1)\u5176\u7eb3\u7c73\u7247\u7684\u7ed3\u6784\u6a21\u578b\u3002<\/p>\n

(g) (h)\u548c(i) Ni-Co-O\u7eb3\u7c73\u7247\u4f4e\u500d\u548c\u9ad8\u500d\u626b\u63cf\u56fe(SEM),(i-1)\u5176\u7eb3\u7c73\u7247\u7684\u7ed3\u6784\u6a21\u578b\u3002<\/p>\n

\u56fe\u4e09\uff1aTEM\u8868\u5f81\u548c\u7ed3\u6784\uff0c\u5143\u7d20\u5206\u6790<\/strong><\/p>\n

\"\"<\/p>\n

(a) (b) (c)(d) (e) \u548c(f)Ni3<\/sub>S2<\/sub>\/CoNi2<\/sub>S4<\/sub>\u7eb3\u7c73\u7247\u7684\u4f4e\u500d\u3001\u9ad8\u500dTEM\u8868\u5f81\u548c\u9009\u533a\u7535\u5b50\u884d\u5c04(SAED)\u5206\u6790\u3002<\/p>\n

(g) (h) (i)\u548c(j)Ni-Co-O\u7eb3\u7c73\u7247\u7684\u4f4e\u500d\u3001\u9ad8\u500dTEM\u8868\u5f81\u53ca\u5176SAED\u5206\u6790\u3002<\/p>\n

(k)\u548c(I)Ni-Co-precursor\u7eb3\u7c73\u7247\u7684TEM\u8868\u5f81\u3002<\/p>\n

(m)(n) (o) \u548c(p)Ni3<\/sub>S2<\/sub>\/CoNi2<\/sub>S4<\/sub>\u7eb3\u7c73\u7247\u7684EDS\u5143\u7d20\u5206\u5e03\u56fe\u3002<\/p>\n

\u56fe\u56db\uff1aNi3<\/sub>S2<\/sub>\/CoNi2<\/sub>S4<\/sub>\/NF\/\/AC\/NF\u975e\u5bf9\u79f0\u7535\u5bb9\u5668\u7684\u7535\u5316\u5b66\u6027\u80fd\u8868\u5f81<\/strong><\/p>\n

\"\"<\/p>\n

(a)\u975e\u5bf9\u79f0\u8d85\u7ea7\u7535\u5bb9\u5668\u5728\u4e0d\u540c\u7535\u4f4d\u7a97\u53e3\u4e0b\u7684CV\u66f2\u7ebf\u3002<\/p>\n

(b) \u975e\u5bf9\u79f0\u8d85\u7ea7\u7535\u5bb9\u5668\u5728\u4e0d\u540c\u626b\u901f\u4e0b\u7684CV\u66f2\u7ebf\u3002<\/p>\n

(c)\u975e\u5bf9\u79f0\u8d85\u7ea7\u7535\u5bb9\u5668\u5728\u4e0d\u540c\u7535\u6d41\u5bc6\u5ea6\u4e0b\u7684\u6052\u6d41\u5145\u653e\u7535\u66f2\u7ebf\u3002<\/p>\n

(d) \u975e\u5bf9\u79f0\u8d85\u7ea7\u7535\u5bb9\u5668\u7684\u500d\u7387\u6027\u80fd\u548c\u5e93\u4f26\u6548\u7387\u56fe\u3002<\/p>\n

(e) \u548c(f)\u6d4b\u8bd5\u6e29\u5ea6\u5bf9\u975e\u5bf9\u79f0\u8d85\u7ea7\u7535\u5bb9\u5668CV\u66f2\u7ebf\u7684\u5f71\u54cd\u3002<\/p>\n

\u56fe\u4e94\uff1aNi3<\/sub>S2<\/sub>\/CoNi2<\/sub>S4<\/sub>\/NF\/\/AC\/NF\u975e\u5bf9\u79f0\u7535\u5bb9\u5668\u673a\u68b0\u6027\u80fd\u3001\u529f\u7387\u5bc6\u5ea6\u3001\u5faa\u73af\u6027\u80fd\u56fe<\/strong><\/p>\n

\"\"<\/p>\n

(a) \u975e\u5bf9\u79f0\u8d85\u7ea7\u7535\u5bb9\u5668\u7684\u673a\u68b0\u67d4\u97e7\u6027\u7814\u7a76\u3002<\/p>\n

(b) \u975e\u5bf9\u79f0\u8d85\u7ea7\u7535\u5bb9\u5668\u4e0e\u5df2\u62a5\u9053\u7684\u8d85\u7ea7\u7535\u5bb9\u5668\u7684\u5bf9\u6bd4Ragone plot\u56fe\u3002<\/p>\n

(c) \u975e\u5bf9\u79f0\u8d85\u7ea7\u7535\u5bb9\u5668\u7684\u5faa\u73af\u7a33\u5b9a\u6027\u6d4b\u8bd5\u3002<\/p>\n

(d) \u8d85\u7ea7\u7535\u5bb9\u5668\u5728LED\u4e0a\u7684\u5e94\u7528\u3002<\/p>\n

\u3010<\/strong>\u603b<\/strong>\u7ed3\u4e0e\u5c55\u671b<\/strong>\u3011<\/strong><\/p>\n

\u8be5\u8bfe\u9898\u7ec4\u901a\u8fc7\u63a7\u5236\u5bf9Ni-Co-precursor\u7684\u786b\u5316\u6761\u4ef6\uff0c\u5de7\u5999\u7684\u5236\u5907\u4e86\u8d85\u8584\u3001\u591a\u5b54\u7eb3\u7c73\u7247\u7f51\u7edc\u81ea\u652f\u6491\u7535\u6781\u3002\u8be5\u79cd\u7ed3\u6784\u5728KOH\u7535\u89e3\u6db2\u4e2d\u62e5\u6709\u9ad8\u7684\u7a33\u5b9a\u6027\u548c\u4f18\u826f\u7684\u5bfc\u7535\u6027\uff0c\u6784\u5efa\u4e86\u5feb\u901f\u3001\u9ad8\u6548\u7684\u7535\u5b50\u548c\u79bb\u5b50\u8f93\u8fd0\u8def\u5f84\u3002\u7ec4\u88c5\u7684\u67d4\u6027\u8d85\u7ea7\u7535\u5bb9\u5668\u62e5\u6709\u6770\u51fa\u7684\u7a33\u5b9a\u6027\uff0c\u673a\u68b0\u67d4\u97e7\u6027\uff0c\u5bbd\u7684\u7535\u538b\u7a97\u53e3\u548c\u9ad8\u7684\u80fd\u91cf\u5bc6\u5ea6\u3002\u4e3a\u65b0\u578b\u9ad8\u6548\u50a8\u80fd\u8bbe\u5907\u7684\u7814\u53d1\u63d0\u4f9b\u4e86\u4e00\u4e2a\u826f\u597d\u7684\u601d\u8def\u3002<\/p>\n

\u3010<\/strong>\u53c2<\/strong>\u8003\u6587\u732e<\/strong>\u3011<\/strong><\/p>\n

\u6587\u7ae0\u94fe\u63a5\uff1aUltrathin and Porous Ni3<\/sub>S2<\/sub>\/CoNi2<\/sub>S4<\/sub>3D-Network Structure for Superhigh Energy Density Asymmetric Supercapacitors<\/a> (Adv. Energy Mater. 2017 10.1002\/aenm.201700983 )<\/p>\n

\u672c\u6587\u7531\u6d4e\u5357\u5927\u5b66\u5f90\u9521\u91d1\u6559\u6388\u6295\u7a3f\uff0c\u6750\u6599\u725b\u7f16\u8f91\u5927\u57ce\u5c0f\u7231\u6574\u7406\u7f16\u8f91\u3002<\/p>\n

\u6295\u7a3f\u4ee5\u53ca\u5185\u5bb9\u5408\u4f5c\u53ef\u52a0\u7f16\u8f91\u5fae\u4fe1\uff1a<\/strong>xiaofire-18<\/strong>\uff0c\u5434\u73ab\uff0c\u6211\u4eec\u4f1a\u9080\u8bf7\u5404\u4f4d\u8001\u5e08\u52a0\u5165\u4e13\u5bb6\u7fa4\u3002<\/strong><\/p>\n

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